| 肾衰丸中大黄素的含量测定 |
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| 引用本文： | 王虎,陈华庭,徐楚鸿.肾衰丸中大黄素的含量测定[J].中国医院药学杂志,2005,25(9):833-835. |
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| 作者姓名： | 王虎 陈华庭 徐楚鸿 |
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| 作者单位： | 华中科技大学同济医学院附属协和医院,湖北,武汉,430022 |
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| 摘 要： | 目的:控制肾衰丸的质量,以保证用药安全有效.方法:用高效液相色谱法对大黄素进行含量测定.结果:大黄素加样回收率为98.86%,RSD为1.73%(n=5),3批样品中大黄素的含量分别为0.412,0.407,0.396 mg/粒.结论:本方法简便,快速,结果可靠,可作为肾衰丸的质量控制手段.
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| 关 键 词： | 大黄素 高效液相色谱 肾衰丸 |
| 文章编号： | 1001-5213(2005)09-0833-03 |
| 收稿时间： | 2004-10-06 |
| 修稿时间： | 2004年10月6日 |
Determination of emodin in Shenshuai pills by RP-HPLC |
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| WANG Hu,CHEN Hua-ting,XU Chu-hong.Determination of emodin in Shenshuai pills by RP-HPLC[J].Chinese Journal of Hospital Pharmacy,2005,25(9):833-835. |
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| Authors: | WANG Hu CHEN Hua-ting XU Chu-hong |
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| Abstract: | OBJECTIVE To control the quality standard and guarantee the effective and safe use of Shenshuai pills. METHODS Emodin of Shenshuai pills was determined by HPLC. RESULTS Average recovery was 98.86% with RSD of 1.73%. The contents of Shenshuai pills in three batches were 0. 412, 0. 407, 0. 396 mg/pill respectively. CONCLUSION The method is simple, reliable and can be used for controlling the quality of Shenshuai pills. |
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| Keywords: | emodin HPLC Shenshuai pill |
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