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竹黄菌发酵液化学成分研究
引用本文:胡居杰,尹 伟,吴培云,梁益敏,王 刚.竹黄菌发酵液化学成分研究[J].安徽中医学院学报,2011,30(6):58-60.
作者姓名:胡居杰  尹 伟  吴培云  梁益敏  王 刚
作者单位:1. 安徽省金寨县人民医院,安徽,金寨,234321
2. 安徽新华学院药学院,安徽,合肥,230038
3. 安徽中医学院药学院,现代中药安徽省重点实验室,安徽,合肥,230031
摘    要:目的研究竹黄菌发酵液的化学成分。方法从竹黄菌发酵液的乙酸乙酯萃取部分运用色谱方法分离纯化化合物,并通过理化性质及波谱数据鉴定化合物的化学结构。结果从竹黄发酵液的乙酸乙酯萃取部分,分离得到6个化合物,分别为:棕榈酸甲酯(1);棕榈酸(2);5α,8α-epidiory-(22E,24R)-ergosta-6,22-dien-3β-ol(3);D-阿洛醇(4);胡萝卜苷(5);4-羟基-苯甲酸(6)。结论所有化合物均为首次从该真菌中分离得到。

关 键 词:竹黄  提取  分离  结构鉴定

Chemical Constituents of Fermentation Liquid of Shiraia bambusicola
HU Ju-jie,YIN Wei,WU Pei-yun,LIANG Yi-min,WANG Gang.Chemical Constituents of Fermentation Liquid of Shiraia bambusicola[J].Journal of Anhui Traditional Chinese Medical College,2011,30(6):58-60.
Authors:HU Ju-jie  YIN Wei  WU Pei-yun  LIANG Yi-min  WANG Gang
Institution:1.The People’s Hospital of Jinzhai County,Anhui Jinzhai 234321,China;2.Department of Pharmacy,Anhui Xinhua College,Anhui Hefei 230038,China;3.Department of Pharmacy,Anhui College of Traditional Chinese Medicine & Anhui Key Laboratory of Modernized Chinese Medicine,Anhui Hefei 230031,China)
Abstract:Objective To study the chemical constituents in the fermentation liquid of Shiraia bambusicola P.Henn.Methods The ethyl acetate extracts in the fermentation liquid of Shiraia bambusicola were isolated and purified by using chromatographic methods.The structures of the constituents were elucidated by physical and chemical properties and spectral data.Results Six compounds were obtained from the ethyl acetate extracts in the fermentation liquid of Shiraia bambusicola,including methylpalmitate(1),palmitate(2),5α,8α-epidiory-(22E,24R)-ergosta-6,22-dien-3β-ol(3),D-allitol(4),Daucosterol(5),and 4-hydroxy benzoic acid(6).Conclusion All the compounds are isolated from the Shiraia bambusicola for the first time.
Keywords:Shiraia bambusicola  extraction  isolation  structure identification
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