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| 直立白薇化学成分研究 | |
| 引用本文： | 袁鹰,张卫东,张川,柳润辉,苏娟,金慧子.直立白薇化学成分研究[J].中国中药杂志,2007,32(18):1895-1897. |
| 作者姓名： | 袁鹰 张卫东 张川 柳润辉 苏娟 金慧子 |
| 作者单位： | 1. 上海交通大学,药学院,上海,200240 2. 上海交通大学,药学院,上海,200240;第二军医大学,药学院,上海,200433 3. 第二军医大学,药学院,上海,200433 |
| 摘 要： | 目的：研究直立白薇的化学成分。方法：利用色谱技术进行分离和纯化,并通过现代光谱方法鉴定其化学结构。结果：分离得到12个化合物,并鉴定了其中的9个,分别为2,4-二羟基苯乙酮(1),2,6-二羟基苯乙酮(2),4-羟基苯甲醇(3),苯甲酸(4),β-香树素乙酸酯(5),棕榈酸(6),β-谷甾醇(7),β-胡萝卜苷(8),白前苷元C-3-O-α-D-吡喃夹竹桃糖基-(1→4)-β-D-吡喃洋地黄毒糖基-(1→4)-α-D-吡喃夹竹桃糖苷(9)。结论：化合物2～8为首次从该植物中分得。 |
| 关 键 词： | 萝藦科 直立白薇 化学成分 |
| 文章编号： | 1001-5302（2007）18-1895-04 |
| 收稿时间： | 3/1/2007 12:00:00 AM |
| 修稿时间： | 2007年3月1日 |
Studies on Chemical constituents from root of Cynanchum atratum |
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| YUAN Ying; ZHANG Wei-dong;; ZHANG Chuan; LIU Run-hui; SU Juan; JIN Hui-zi.Studies on Chemical constituents from root of Cynanchum atratum[J].China Journal of Chinese Materia Medica,2007,32(18):1895-1897. | |
| Authors: | YUAN Ying; ZHANG Wei-dong;; ZHANG Chuan; LIU Run-hui; SU Juan; JIN Hui-zi |
| Institution: | 1. School of Pharmacy, Shanghai Jiaotong University, Shanghai 200240, China; 2. School of Pharmacy, Second Military Medical University, Shanghai 200433, China |
| Abstract: | OBJECTIVE: To study the chemical constituents from the roots and rhizome of Cynanchum atratum. METHOD: The chemical constituents were isolated and repeatedly purified by silica gel chromatography and the structures were elucidated by the NMR spectra and physicochemical properties. RESULT: Twelve compounds were obtained and nine of them were identified as 2, 4-dihyroxyacetophe none (1), 2, 6-dihyroxyacetophenone (2), 4-hydroxybenzenemethanol (3), benzoic acid (4), beta-amyrin acetate (5), palmitic acid (6), beta-sitosterol (7), beta-daucosterol (8), glaucogenin C-3-O-alpha-D-oleandropyranosyl-(1 --> 4)-beta-D-digitoxopyranosyl-(1 -->4)-alpha-D-oleandropyranoside (9). CONCLUSION: Seven compounds were obtained from C. atratum for the first time. |
| Keywords: | Asclepiadaceae Cynanchum atratum chemical constituents |
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