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1.
用傅里叶红外光谱(FTIR)法研究了双酚S环氧树脂和甲溴双酚A环氧树脂分别与二胺基二苯砜在恒温条件下的固化反应动力学,得出了各反应的表观活化能。  相似文献   

2.
通过二甲基甲酰胺的等离子体聚合作用,对聚乙烯膜进行表面改性。研究了等离子体工艺参数对聚合物膜沉积速度的影响,用FTIR、XPS分析了聚合物膜的组成结构,测定了改性聚乙烯膜的接触角和表面。  相似文献   

3.
以聚乙烯-马来酸酐接枝共聚物为基础,合成马来酸型的碱金属(Na和K)、碱土金属(Mg和Ca)及过渡金属(Zn和Cd)离聚体,详细研究了它们在不同中的度下的FTIR光谱的变化规律,探讨它们的形成的机理及其聚集态的结构膜型。  相似文献   

4.
用萃取-层析法分离出了南京管输油馏分中的含氮化合物,用GC-MS和FTIR对含氮化合物组分作了定性鉴定,所得结果与API离子交换分离法作了比较。  相似文献   

5.
对20~86岁正常中老年520例的部分呼气流量-容积(PEFV)曲线及有关肺功能指标作了测定,并用多元逐步回归分析法建立了功能残气位呼气流量(VFRC)、用容积校正的VFRC/FVC、各肺容积流量V75、V50、V25以及比时间常数Sτ75、Sτ50、Sτ25的回归方程。VFRC随年龄增长而下降;经容积校正后的VFRC/FVC与年龄的相关性下降。将回归方程用正常人参数作回代检查证明其正确性。结果提示PEFV曲线方法简便,具有理论研究和临床应用意义。  相似文献   

6.
利用差热扫描量热计(DSC)、红外光谱仪(FTIR)、扫描电镜(SEM)和力学性能测试等手段研究了PMMA/PVC二元共混体系的形态结构和性能。结果表明,PMMA和PVC之间存在较强的特殊相互作用力,在一定配比范围内为一良好相容体系,这与Fox方程和Hamada修正方程估算的结果吻合。  相似文献   

7.
以Shooting法为基础,研究了吸收、增益和晶体厚度对光折变晶体中逆向二波混合的影响,对近似计算所引起的误差进行了讨论。对晶体表面内反射对光束透过率的影响,提出了以Shooting法为基础的自洽计算方法,计算了透过率与晶体表面反射率的关系。  相似文献   

8.
利用磷酸对高岭土进行处理,制取不同含磷量的活性基质,然后与分子筛、填充物等组合成FCC催化剂。在用FTIR技术和MAT试验等催化剂表征手段对其表征之后,发现酸性,酸密度和强度等与催化剂的裂化性能有很大关系;所制5种不同含磷量催化剂的酸性特征随含磷量的变化而较有规律地变化。  相似文献   

9.
PA1010/丁基橡胶磺酸锌盐共混体系的DSC、FTIR、固体NMR结果表明两组份之间存在强的相互作用,DMA结果表明随锌盐的比例增加,两组份相容性增加,并产生混合新相。PA1010/丁基橡胶磺酸钠盐共混体系中两组份之间的相互作用不明显,相容性较差。SEM结果与上述结果完全吻合。  相似文献   

10.
研究了新型As_2Se_3-GeTe-Cul系统玻璃形成区,制备了一系列不同CuI或GeTe含量的玻璃,并测定其转变温度、密度、显微硬度、断裂韧性、膨胀系数、红外透过率和反射率。结果表明:该系统玻璃的形成范围很大,玻璃转变温度在170~230℃,显微硬度在130~190kg/mm ̄2,断裂韧性在0.30~0.50MN/m ̄(3/2),膨胀系数在145×10 ̄(-7)~215×10 ̄(-7)℃,红外透过截止波长超过19μm,反射率在20%左右。并初步从结构的观,或讨论了玻璃性质变化的规律。  相似文献   

11.
FOR anesthesiologis s ,treatingpostoperativepainhas alwaysbeen a problem.Althoughopioidshave been provedtobe effective,theirsideeffectscouldnotbeignored.With thedevelopmentofscienceand pharmacology,many drugs with aspectsof satisfactoryanalgesicefficacyand couldbe welltoleratedby patientshave been developed.And lornoxicamisone of them, which isa non-steroidalanti-inflammatorydrug (NSAID ), with analgesic, anti-infl-ammatory,andantipyreticproperties.Itseliminationhalf-time(3 to 5 hours) isle…  相似文献   

12.
CASE HISTORY A female patient, 46 years old, head of the foreign affairs department of a certain university in Beijing, paid her first visit on October 9, 2006, with the chief complaint of vomiting for one month. She got vomiting after meals in early September. Before that, she had discomfortable sensation in the stomach due to angry with others, but she didn't pay much attention. Later, it developed into vomiting after eating. After the vomiting, the discomfort would be relieved, but with slight hypodynamia. She was once diagnosed as having 'neurogenic vomiting'. Having taken some western and Chinese drugs, the above symptoms were a little bit improved, but she would have nausea upon eating and with regurgitation. Because of the fear for vomiting, she did not dare to have food intake, with body weight reduction of 6 kilos in one month.  相似文献   

13.
Radiotherapy and chemotherapy are the important modern medical therapies for malignant tumors,yet they can also bring about serious local and systemic toxic side reactions so to decrease the patient;'s life quality,manifested by a series of consumptive symptoms.Having engaged in the combined work of Chinese and western medicine for nearly 50 years,the research fellow Qiu Baoguo in Henan Provincial Academy of TCM has developed his unique views on the TCM study of consumptive syndromes.The author of this essay had once the fortune tO follow Dr.Qiu in clinic,and specially would like to introduce in the following Dr.Qiu's experience in treating consumptive syndromes after radio-chemotherapies for patients with malignant tumor.  相似文献   

14.
OBJECTIVE: To observe therapeutic effects of the comprehensive therapy of acupuncture-moxibustion and Chinese Tuina for treatment of insomnia due to deficiency of both the heart and spleen. METHODS: 92 cases were divided randomly into the treatment group (treated by acupuncture-moxibustion and Chinese Tuina) and the control group (treated by acupuncture-moxibustion). RESULTS: The therapeutic effect of the treatment group was obviously superior to that of the control group (the CHI2 test showed P < 0.01). CONCLUSIONS: The comprehensive therapy of acupuncture-moxibustion and Chinese Tuina can give marked therapeutic effects for treatment of insomnia due to deficiency of both the heart and spleen.  相似文献   

15.
16.
Objective: To investigate if there are the CK-19, PDX-1, Nestin, Ngn3 positive cells in the donor islets of different purity in rats. Methods: Thirty male adult SD rats were randomly divided into 3 groups. Islets were isolated using digestion by ductal injection of collagenase. Group Ⅰ (n=10): Separating cell preparations were not purified, Group Ⅱ(n=10): Islet sediment was purified with 25% Ficoll400 ,Group Ⅲ (n=10): Islet sediment was purified with 25% and 11% Ficoll-400. The levels of protein of CK-19, PDX-1, Nestin and Ngn3 were detected by immunohistochemistry and the mRNA of CK-19, PDX-1, Nestin, Ngn3 was amplified by RT-PCR. Results: After two different purification methods applied, three islet preparations of different purities were obtained. The difference of islet purity was significant among various groups (P<0.05). Compared with group Ⅱ and group Ⅲ,the protein and mRNA of CK-19, PDX-1, Nestin,Ngn3 were both higher in group Ⅰ; group Ⅲ was poorly expressed. Conclusions: The three different islet purity donor islet have different CK-19, PDX-1, Nestin, Ngn3 positive cells within them, indicating that there are some islet stem cells in the purified donor islet.  相似文献   

17.
Dr.Zhang Ren,the chief physician,is the chairman of Shanghai Acupuncture and Moxibustion Association.Having been engaged in medicine for about 40 years,he is experienced in treating various intractable diseases.In his long years of clinical practice,he advocates taking the TCM differentiation as the basis to seek for the acupuncture method for treatment of modern intractable diseases.The author of this essay had the fortune to follow Dr.Zhang in study.The following is a summary of Dr.Zhang's experience in the acupuncture treatment for different intractable diseases with the same therapeutic principle.  相似文献   

18.
In treating chronic nephropathy,Luo Lingjie,a chief physician,pays attention to regulating the balance between yin and yang,treating infection if present,and removing pathogenic factors.He prescribes gentle drugs and uses carefully strongly warming-tonifying ones,emphasizes the importance of persuading the patient to persist in treatment with medication and nurse one's health for recuperation,and is good at combined use of TCM and western medicine therapy and brings the merits of various therapies into full play,with obvious theraoeutic effects.  相似文献   

19.
Objective: To observe the therapeutic effects in acupunture treatment of primary dysmenorrhea combined with spinal Tui Na, and study its mechanism. Methods: Thirty cases of the treatment group were treated by acupuncture combined with spinal Tui Na, and thirty cases in the control group were treated by routine acupuncture. Results: The total effective rate was 93.3% in the treatment group, and 73.3% in the control group, with a significant difference between the two groups (P<0.05). Conclusions: Acupuncture combined with spinal Tui Na has good prospects for treatment of primary dysmenorrhea.  相似文献   

20.
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