| 一测多评法同时测定胃力康颗粒中7种成分的含量 |
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| 引用本文： | 柴士伟,屠亚茹,王兴蕊,刘二伟,常艳旭,何俊. 一测多评法同时测定胃力康颗粒中7种成分的含量[J]. 天津中医药, 2016, 33(4): 241-244 |
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| 作者姓名： | 柴士伟 屠亚茹 王兴蕊 刘二伟 常艳旭 何俊 |
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| 作者单位： | 天津中医药大学, 天津 300193;天津中医药大学第一附属医院, 天津 300193,天津中医药大学, 天津 300193,天津中医药大学, 天津 300193,天津中医药大学, 天津 300193,天津中医药大学, 天津 300193,天津中医药大学, 天津 300193;天津市现代中药重点实验室-省部共建国家重点实验室培育基地, 天津 300193 |
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| 基金项目： | 国家科技重大专项重大新药创制项目(2013ZX09402201)。 |
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| 摘 要： | [目的]建立可用于胃力康颗粒中7种成分含量测定的一测多评法。[方法]采用超高效液相色谱(UPLC),以芍药苷为内参物,确定芦丁、柚皮苷、迷迭香酸、丹酚酸B、大黄素-8-O-β-D-葡萄糖苷、甘草酸的相对校正因子,通过相对校正因子计算各成分的含量;同时比较10批胃力康颗粒一测多评法的计算值与外标法测定结果的差异。[结果]建立了胃力康颗粒中7种成分一测多评的含量测定方法,10批胃力康颗粒中7种成分采用一测多评法测定与外标法测定结果无明显差异。[结论]本实验建立的一测多评法可用于胃力康颗粒中7种成分的含量测定,方法快速、准确,可用于胃力康颗粒的质量控制。
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| 关 键 词： | 胃力康颗粒 一测多评法 超高效液相色谱法 质量控制 |
| 收稿时间： | 2015-11-30 |
Simultaneous determination of seven constituents in Wenlikang granules by quantitative analysis of multi-components by single marker |
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| CHAI Shi-wei,TU Ya-ru,WANG Xing-rui,LIU Er-wei,CHANG Yan-xu and HE Jun. Simultaneous determination of seven constituents in Wenlikang granules by quantitative analysis of multi-components by single marker[J]. Tianjin Journal of Traditional Chin Medicine, 2016, 33(4): 241-244 |
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| Authors: | CHAI Shi-wei TU Ya-ru WANG Xing-rui LIU Er-wei CHANG Yan-xu HE Jun |
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| Affiliation: | Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;The First Affiliated Hospital of Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China,Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China,Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China,Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China,Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China and Tianjin University of Traditional Chinese Medicine, Tianjin 300193, China;Tianjin State Key Laboratory of Modern Chinese Medicine-Province and Ministry Co-established State Key Laboratory Cultivation Base, Tianjin 300193, China |
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| Abstract: | |
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| Keywords: | Weilikang granules quantitative analysi of multi-components by single marker UPLC quality control |
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