| 高效液相色谱法测定银蒲解毒片中蒙花苷含量 |
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| 引用本文： | 黎钰铃,覃容芳,张承灿. 高效液相色谱法测定银蒲解毒片中蒙花苷含量[J]. 中国中医药信息杂志, 2008, 15(12): 55-56 |
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| 作者姓名： | 黎钰铃 覃容芳 张承灿 |
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| 作者单位： | 广西玉林制药有限责任公司,广西,玉林,537001 |
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| 摘 要： | 目的建立银蒲解毒片中蒙花苷的含量测定方法。方法采用高效液相色谱法，Agilent Eclipse XDB-C18色谱柱（4．6mm×250mm，5μm），流动相为甲醇-4％冰醋酸水溶液（47：53），检测波长334nm。结果蒙花苷线性范围为2．24—44．8μg（r=0．9991）；平均回收率为97．8％，RSD=1．52％。结论方法可靠，简单可行，为控制银蒲解毒片的内在质量提供了依据。
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| 关 键 词： | 银蒲解毒片 蒙花苷 高效液相色谱法 |
Content Determination of Buddleoside in Compound Yinpujiedu Tablet by HPLC |
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| LI Yu-ling,QIN Rong-fang,ZHANG Cheng-can. Content Determination of Buddleoside in Compound Yinpujiedu Tablet by HPLC[J]. Chinese Journal of Information on Traditional Chinese Medicine, 2008, 15(12): 55-56 |
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| Authors: | LI Yu-ling QIN Rong-fang ZHANG Cheng-can |
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| Affiliation: | LI Yu-ling,QIN Rong-fang,ZHANG Cheng-can (Guangxi Yulin Pharmaceutical Co.Ltd.,Yulin 537001,China) |
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| Abstract: | Objective To establish a method for content determination of Buddleoside in Compound Yinpujiedu Tablet. Method HPLC method, Agilent Eclipse XDB-C18 column （4.6 mm×250 mm, 5 μm） was used, mobile phase was methanol-4% glacial acetic acid （47 ： 53）, and the detecting wavelength was set at 334 nm. Result The standard curve was linear within the range of 2.24-44.8μg. The average recovery and RSD were 97.8% and 1.52%, respectively. Conclusion This method is accurate, reliable, and can provide a scientic index for quality control of Compound Yinpujiedu Tablet. |
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| Keywords: | Compound Yinpujiedu Tablet Buddleoside HPLC |
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