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Evaluation of dental composite shrinkage and leakage in extracted teeth using X-ray microcomputed tomography
Authors:Diana N. Zeiger   Jirun Sun   Gary E. Schumacher  Sheng Lin-Gibson  
Affiliation:aPolymers Division, National Institute of Standards and Technology, Gaithersburg, MD, USA;bPaffenbarger Research Center, American Dental Association Foundation, Gaithersburg, MD, USA
Abstract:ObjectiveUse X-ray microcomputed tomography (μCT), to test the hypothesis that composite shrinkage and sites of potential leakage in human teeth are non-uniformly distributed and depend on cavity geometry and C-factor.MethodsTwo holes of equal volume but different dimensions were drilled into the exposed dentin of extracted human molars. The cavities were filled with composite and teeth were scanned, before and after curing, using μCT. Three-dimensional (3D) reconstructions of the data were prepared and analyzed using image analysis software.Results3D reconstructions showed that cavity geometry did not affect the polymerization shrinkage. The shrinkage for all restorations was 2.66 ± 0.59%, and cavity dimensions did not affect the volume lost, either in quantity or location on the sample. Potential leakage sites were identified by gap formations and found to be non-uniformly distributed along the tooth–composite interface. Leakage in regions calculated by μCT was confirmed by visualization of sectioned samples with confocal laser scanning microscopy.SignificanceμCT evaluation will add tremendous value as part of a suite of tests to characterize various properties of dental materials. The non-uniform distribution of potential leakage sites about the cavities that was determined by μCT emphasizes the inadequacy of traditional methods of determining leakage, which are capable of analyzing only limited areas. Additionally, μCT evaluation can produce quantitative analyses of shrinkage and leakage, compared to the conventional methods, which are qualitative or semi-quantitative. Finally, experimentally determined shrinkage and leakage of composite in extracted teeth agrees with the results of similar experiments in model cavities, confirming the validity of those models.
Keywords:Dental materials   Image analysis   Leakage   Polymerization shrinkage   Resin composites   Extracted teeth   X-ray microcomputed tomography
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