| 舒胸脉冲控释滴丸中阿魏酸和羟基红花黄色素A的测定 |
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| 引用本文： | 陈卉,陈燕忠,谢清春,申楼,班俊峰,冯思欣,赵雪晴,梁兆丰,林世源,吕竹芬.舒胸脉冲控释滴丸中阿魏酸和羟基红花黄色素A的测定[J].中国实验方剂学杂志,2013,19(10):92-94. |
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| 作者姓名： | 陈卉 陈燕忠 谢清春 申楼 班俊峰 冯思欣 赵雪晴 梁兆丰 林世源 吕竹芬 |
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| 作者单位： | 广东药学院药物研究所/广东省药物新剂型重点实验室,广州,510006 |
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| 基金项目： | 广东省自然科学基金项目(S2011010002485) |
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| 摘 要： | 目的:探索HPLC测定舒胸脉冲控释滴丸中阿魏酸和羟基红花黄色素A的含量.方法:采用Kromasil C18色谱柱(4.6 mm×250 mm,5μm),以甲醇-0.01 ool·L-1磷酸二氢钾水溶液(22:78)用磷酸调节pH 3.0为流动相,流速1.0 mL·min-,检测波长403,322 nm,柱温30℃.结果:阿魏酸在1.409 ～90.16 mg·L-1回归方程为A=0.8206C-0.2874(r=0.9999),平均回收率为99.43％,RSD3.42％(n=6);羟基红花黄色素A在4.035 ～ 258.3 mg.L-1,回归方程为A =0.412 7C-0.487 8(r=0.999 7),平均回收率为100.03％,RSD 3.55％(n=6).结论:该方法操作简便,准确,重复性良好,可用于舒胸脉冲控释滴丸的质量控制.
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| 关 键 词： | 舒胸脉冲控释滴丸 高效液相色谱 阿魏酸 羟基红花黄色素A 含量测定 |
| 收稿时间： | 9/7/2012 12:00:00 AM |
Study on Determination of Ferulic Acid and Hydroxy Safflower Yellow A in Shuxiong Pulsatile Controlled-release Dropping Pill |
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| CHEN Hui,CHEN Yan-zhong,XIE Qing-chun,SHEN Lou,BAN Jun-feng,FENG Si-xin,ZHAO Xue-qing,LIANG Zhao-feng,LIN Shi-yuan and LV Zhu-fen.Study on Determination of Ferulic Acid and Hydroxy Safflower Yellow A in Shuxiong Pulsatile Controlled-release Dropping Pill[J].China Journal of Experimental Traditional Medical Formulae,2013,19(10):92-94. |
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| Authors: | CHEN Hui CHEN Yan-zhong XIE Qing-chun SHEN Lou BAN Jun-feng FENG Si-xin ZHAO Xue-qing LIANG Zhao-feng LIN Shi-yuan and LV Zhu-fen |
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| Institution: | Institute of Material Medica/Guangdong Provincial Key Laboratory of Advanced Drug Delivery, Guangdong Pharmaceutical College, Guangzhou 510006, China;Institute of Material Medica/Guangdong Provincial Key Laboratory of Advanced Drug Delivery, Guangdong Pharmaceutical College, Guangzhou 510006, China;Institute of Material Medica/Guangdong Provincial Key Laboratory of Advanced Drug Delivery, Guangdong Pharmaceutical College, Guangzhou 510006, China;Institute of Material Medica/Guangdong Provincial Key Laboratory of Advanced Drug Delivery, Guangdong Pharmaceutical College, Guangzhou 510006, China;Institute of Material Medica/Guangdong Provincial Key Laboratory of Advanced Drug Delivery, Guangdong Pharmaceutical College, Guangzhou 510006, China;Institute of Material Medica/Guangdong Provincial Key Laboratory of Advanced Drug Delivery, Guangdong Pharmaceutical College, Guangzhou 510006, China;Institute of Material Medica/Guangdong Provincial Key Laboratory of Advanced Drug Delivery, Guangdong Pharmaceutical College, Guangzhou 510006, China;Institute of Material Medica/Guangdong Provincial Key Laboratory of Advanced Drug Delivery, Guangdong Pharmaceutical College, Guangzhou 510006, China;Institute of Material Medica/Guangdong Provincial Key Laboratory of Advanced Drug Delivery, Guangdong Pharmaceutical College, Guangzhou 510006, China;Institute of Material Medica/Guangdong Provincial Key Laboratory of Advanced Drug Delivery, Guangdong Pharmaceutical College, Guangzhou 510006, China |
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| Abstract: | |
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| Keywords: | Shuxiong pulsatile controlled-release dropping pill HPLC ferulic acid hydroxy safflower yellow A content determination |
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