| 血竭中5-羟基-7-甲氧基黄烷的含量测定 |
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| 引用本文： | 付梅红,方婧,杨洪军,王祝举,唐力英,黄璐琦,杨岚,张东. 血竭中5-羟基-7-甲氧基黄烷的含量测定[J]. 中国中药杂志, 2010, 35(23): 3192-3193 |
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| 作者姓名： | 付梅红 方婧 杨洪军 王祝举 唐力英 黄璐琦 杨岚 张东 |
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| 作者单位： | 中国中医科学院,中药研究所,北京,100700 |
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| 基金项目： | 澳门特别行政区科学技术发展基金项目(046/2006/A) |
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| 摘 要： | 目的:建立血竭药材中有效成分5-羟基-7-甲氧基黄烷的HPLC含量测定方法。方法:Dikma Diamonsil C18色谱柱(4.6 mm×150 mm,5μm),流动相为乙腈-水(60∶40),检测波长210 nm,柱温30℃,流速1 mL.min-1。结果:5-羟基-7-甲氧基黄烷在0.01~0.10μg呈良好线性关系,r=0.999 9。平均回收率100.1%(n=6)。结论:该方法简便快速、结果准确,可用于检测血竭药材中有效成分5-羟基-7-甲氧基黄烷的含量。
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| 关 键 词： | 血竭 5-羟基-7-甲氧基黄烷 HPLC 含量测定 |
| 收稿时间： | 2010-02-26 |
Determination of 5-hydroxy-7-methoxyflavan in Daemonorops draco by HPLC |
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| FU Meihong,FANG Jing,YANG Hongjun,WANG Zhuju,TANG Liying,HUANG Luqi,YANG Lan and ZHANG Dong. Determination of 5-hydroxy-7-methoxyflavan in Daemonorops draco by HPLC[J]. China Journal of Chinese Materia Medica, 2010, 35(23): 3192-3193 |
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| Authors: | FU Meihong FANG Jing YANG Hongjun WANG Zhuju TANG Liying HUANG Luqi YANG Lan ZHANG Dong |
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| Affiliation: | Institute of Chinses Materia Medica, China Academy of Traditional Chinese Medicine, Beijing 100700, China;Institute of Chinses Materia Medica, China Academy of Traditional Chinese Medicine, Beijing 100700, China;Institute of Chinses Materia Medica, China Academy of Traditional Chinese Medicine, Beijing 100700, China;Institute of Chinses Materia Medica, China Academy of Traditional Chinese Medicine, Beijing 100700, China;Institute of Chinses Materia Medica, China Academy of Traditional Chinese Medicine, Beijing 100700, China;Institute of Chinses Materia Medica, China Academy of Traditional Chinese Medicine, Beijing 100700, China;Institute of Chinses Materia Medica, China Academy of Traditional Chinese Medicine, Beijing 100700, China;Institute of Chinses Materia Medica, China Academy of Traditional Chinese Medicine, Beijing 100700, China |
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| Abstract: | |
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| Keywords: | Daemonorops draco 5-hydroxy-7-methoxyflavan HPLC quantitative determination |
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