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| 果上叶挥发性成分研究 | |
| 引用本文： | 盛世昌,王道平,刘建华,高玉琼,刘文炜,李计龙. 果上叶挥发性成分研究[J]. 中国实验方剂学杂志, 2011, 17(3): 80-82 |
| 作者姓名： | 盛世昌 王道平 刘建华 高玉琼 刘文炜 李计龙 |
| 作者单位： | 1. 贵州大学,贵阳,550025;贵州省生物技术研究开发基地,贵阳,550002 2. 贵州省中国科学院天然产物化学重点实验室,贵阳,550009 3. 贵州省生物技术研究开发基地,贵阳,550002 |
| 基金项目： | 贵州专项资金项目资助[黔科合院所创能(2009)4010] |
| 摘 要： | 目的:研究果上叶中的挥发性成分。方法:利用有机溶剂-水蒸气蒸馏法提取果上叶挥发油,用GC-MS进行测定,结合计算机检索技术对分离化合物进行结构鉴定,应用色谱峰面积归一化法计算各成分的相对百分含量。结果:分离鉴定出38种化学成分,占挥发油总量91.448%,其中含量大于2%的分别为Z-9-十八烯醛18.075%、2,4-二叔丁基苯酚3.264%、棕榈酸5.413%、油酸25.079%、二十三烷6.344%、二十四烷3.768%、1-十八烯酸单甘油酯2.146%、亚油酸甘油酯4.953%、二十五烷4.332%、二十六烷3.387%、二十七烷3.841%、二十八烷3.102%。结论:本文采用气相色谱-质谱联用法对果上叶中的挥发性成分进行研究。 |
| 关 键 词： | 果上叶 水蒸气蒸馏 挥发性成分 气相色谱-质谱联用 |
| 收稿时间： | 2010-08-09 |
Determination of Chemical Constituents of Volatile Oil from Bulbophyllum odoratissimum |
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| SHENG Shi-chang,WANG Dao-ping,LIU Jian-hu,GAO Yu-qiong,LIU Wen-wei and LI Ji-long. Determination of Chemical Constituents of Volatile Oil from Bulbophyllum odoratissimum[J]. China Journal of Experimental Traditional Medical Formulae, 2011, 17(3): 80-82 | |
| Authors: | SHENG Shi-chang WANG Dao-ping LIU Jian-hu GAO Yu-qiong LIU Wen-wei LI Ji-long |
| Affiliation: | SHENG Shi-chang1,2,WANG Dao-ping3,LIU Jian-hua2,GAO Yu-qiong2,LIU Wen-wei1,LI Ji-long1,2(1.Guizhou university,Guiyang 550025,China,2.Guizhou Institute of Biotechnology Research and Development,Guiyang 550002,3.Key Laboratory of Natural Product Chemistry of the Chinese Academy of Sciences,Guiyang 550009,China) |
| Abstract: | Objective:To study the chemical constituents of the volatile oil from Bulbophyllum odoratissi-mum.Method: The chemical compositions of the volatile oil of the plants which were obtained by organic-steam distillation with hexane were analyzed by GC-MS.The constituents were identified by their mass spectra.The rela-tive percentage of the oil constituents was calculated from the GC peak areas.Result: Thirty-eight kinds of chemical components were identified from B.odoratissimum.The amount of the identified com... |
| Keywords: | Bulbophyllum odoratissimum steam distillation volatile oil GC-MS |
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