| 气相色谱检测水产品中有机氯类农药残留 |
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| 引用本文： | 宋鑫,杭学宇,王芹,王露,冯晓青,徐瑞,茅力.气相色谱检测水产品中有机氯类农药残留[J].国际检验医学杂志,2016(6):733-735. |
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| 作者姓名： | 宋鑫 杭学宇 王芹 王露 冯晓青 徐瑞 茅力 |
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| 作者单位： | 1. 南京医科大学公共卫生学院，江苏南京 211166; 淮安市疾病预防控制中心，江苏淮安 223001;2. 淮安市疾病预防控制中心,江苏淮安,223001;3. 南京医科大学公共卫生学院,江苏南京,211166 |
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| 基金项目： | 淮安市科技局科技发展计划基金项目(HAS2015030)；2015年度淮安市疾控系统预防医学科研课题项目(hayf201520)。 |
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| 摘 要： | 目的建立气相色谱定量测定水产品中16种有机氯类混合农药残留的方法。方法样品由乙腈提取,以氨基固相萃取柱(Carb/NH_2)净化,经气相色谱检测分析。结果 16种化合物在0.05~1.00mg/L内线性关系良好(r0.998),各有机氯的检出限为0.04~0.31μg/kg(S/N=3)。在加标水平为50、100、200μg/kg时,该方法的回收率为72.6%~115.2%,相对标准偏差为0.6%~7.5%。结论该研究建立的方法选择性好、灵敏度高,适用于水产品中有机氯类农药的多残留痕迹测定。
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| 关 键 词： | 气相色谱 水产品 有机氯 |
Determination of organochlorine pesticide in aquatic products by gas chromatography |
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| Abstract: | Objective A method for quantitative determination of 16 kinds of organochlorine pesticide (OCPs) in aquatic prod-ucts by gas chromatography (GC)was established .Methods The sample was extracted by acetonitrile ,purified by Carb/NH2 ,and then determined by GC .Results The linear relations of 16 kinds of OCPs were good at 0 .05 - 1 .00 mg/L(r> 0 .998) .The limit of detection of OCPs was in the range of 0 .04 - 0 .31 μg /kg(S/N = 3) .When the standard levels were 50 ,100 ,200 μg /kg ,the recovery rates were 72 .6% - 115 .2% ,the relative standard deviations were 0 .6% - 7 .5% .Conclusion The method established in this stud-y is applied to the determination of 16 kinds of OCPs in real samples with satisfactory results . |
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| Keywords: | gas chromatography aquatic products organochlorine pesticide |
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