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火焰原子吸收光谱法测定鸡矢藤中微量元素
引用本文:吕瑞,石兴丽. 火焰原子吸收光谱法测定鸡矢藤中微量元素[J]. 世界科学技术-中医药现代化, 2013, 15(2): 264-266
作者姓名:吕瑞  石兴丽
作者单位:绵阳师范学院化学与化学工程学院,绵阳,621000
基金项目:四川省教育厅重点科研项目(13ZA0112):基于Ru(bpy)32+—染料电化学发光共振能量转移研制高灵敏度的DNA 生物化学传感器,负责人:黄宝美。
摘    要:目的:测定鸡矢藤中微量元素的含量.方法:采用浓硝酸-高氯酸(4:1)的混合溶液对样品进行消解,火焰原子吸收光谱法测定鸡矢藤中微量元素(Fe,Cu,Zn,Mn)的含量.结果:鸡矢藤中Fe,Cu,Zn,Mn含量依次为493.3,6.925,82.33,66.42 μg·g-1,各元素含量由高到低的顺序依次为Fe>Zn>Mn>Cu;方法的平均回收率为100.4%.结论:鸡矢藤中含有较为丰富的Fe,Cu,Zn,Mn,测定结果为鸡矢藤药理作用的研究提供了数据参考.

关 键 词:原子吸收光谱法  鸡矢藤  微量元素
收稿时间:2012-07-28
修稿时间:2013-04-19

Determination of Trace Elements in Paederia Scandens by Flame Atomic Absorption Spectrometry
Lv Rui and Shi Xingli. Determination of Trace Elements in Paederia Scandens by Flame Atomic Absorption Spectrometry[J]. World Science and Technology—Modernization of Traditional Chinese Medicine and Materia Medica, 2013, 15(2): 264-266
Authors:Lv Rui and Shi Xingli
Affiliation:College of Chemistry and Chemical Engineering, Mianyang Normal University, Mianyang 621000, China
Abstract:This study was aimed to determine trace elements in Paederia scandens. The nitric acid and perchloric acid (4:1) mixture was applied to digest the sample. And flame atomic absorption spectroscopy (FAAS) was used to determine the content of trace elements (i.e., Fe, Cu, Zn, Mn) in P. scandens. The result showed that the contents of Fe, Cu, Zn, Mn in P. scandens were 493.3, 6.925, 82.33, 66.42 g·g-1, respectively. The element content of each in high-to-low order was Fe > Zn > Mn > Cu. The average recovery rate was 100.4%. It was revealed that this method is simple and accurate. It was concluded that trace elements (i.e., Fe, Cu, Zn, Mn) in P.scandens is rich. It has provided some useful information for the further pharmacological studies of P. scandens.
Keywords:Atomic absorption spectrometry   Paederia scandens   trace elements
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