| 青藤碱凝胶的制备及质量控制 |
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| 引用本文： | 张先洲,潘细贵,罗顺德,薛承斌,蔡海燕. 青藤碱凝胶的制备及质量控制[J]. 中国药房, 2003, 14(5): 275-277 |
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| 作者姓名： | 张先洲 潘细贵 罗顺德 薛承斌 蔡海燕 |
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| 作者单位： | 武汉大学人民医院药学部,武汉市,430060 |
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| 摘 要： | 目的 :探讨青藤碱凝胶的制备及质量控制标准。方法 :以卡波姆为辅料制备青藤碱凝胶剂 ,采用薄层色谱法及紫外分光光度法鉴别青藤碱 ;用反相高效液相色谱法测定凝胶中青藤碱的含量。结果 :处方设计合理 ,制备方法简便 ,方法平均回收率为(99 6±1 3) %。结论 :本方法操作简便、快速 ,检测结果准确 ,可作为青藤碱凝胶的制备和质量控制方法。
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| 关 键 词： | 青藤碱凝胶 制备 质量标准 |
| 文章编号： | 1001-0408(2003)05-0275-03 |
| 修稿时间： | 2002-07-09 |
Studies on the Preparation and Quality Standards for Sinomenine Gel |
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| ZHANG Xianzhou,PAN Xigui,LUO Shunde,XUE Chengbin,CAI Haiyan. Studies on the Preparation and Quality Standards for Sinomenine Gel[J]. China Pharmacy, 2003, 14(5): 275-277 |
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| Authors: | ZHANG Xianzhou PAN Xigui LUO Shunde XUE Chengbin CAI Haiyan |
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| Abstract: | OBJECTIVE:To develop a preparation and quality control method for sinomenine gel.METHODS:Sinomenine gel was prepared with carpol971as base.TLC and UV were employed for identification of sinomenine.Sinomenine was deterˉmined by RP-HPLC.RESULTS:The TLC identification was highly specific and the spots were clear.Recovery was99.6%±1.3%.CONCLUSION:This paper provides a rapid,convenient and accurate method which is suitable for preparation and quality control for sinomenine gel. |
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| Keywords: | sinomenine gel preparation quality standard |
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