| 固精片质量标准的研究 |
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| 引用本文： | 王玉巧,陈鹏,熊莉. 固精片质量标准的研究[J]. 中成药, 2005, 27(9): 1027-1029 |
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| 作者姓名： | 王玉巧 陈鹏 熊莉 |
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| 作者单位： | 湖北省暨武汉市中药现代化工程技术研究中心,湖北,武汉,430052 |
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| 摘 要： | 目的:建立了固精片的质量标准(乳香、香附、木香等).方法:采用TLC法对处方中乳香、香附、木香进行鉴别;用HPLC法测定木香烃内酯的含量.结果:薄层斑点清晰,专属性强.含量测定线性关系良好,平均回收率为99.1%,RSD为1.25%(n=5).结论:该方法简便准确,重现性好,可作为该制剂的质量控制.
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| 关 键 词： | 固精片 木香烃内酯 质量标准 |
| 文章编号： | 1001-1528（2005）09-1027-03 |
| 收稿时间： | 2004-09-03 |
| 修稿时间： | 2004-09-03 |
Quality standard for Gujing Tablets |
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| WANG Yu-qiao,CHEN Peng,XIONG Li. Quality standard for Gujing Tablets[J]. Chinese Traditional Patent Medicine, 2005, 27(9): 1027-1029 |
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| Authors: | WANG Yu-qiao CHEN Peng XIONG Li |
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| Abstract: | AIM: To establish the quality standard for Gujing Tablets (Olibanum, Rhizoma Cyperi, Radix Aucklandia, etc.). METHODS: Olibanuln, Rhizoma Cyperi, Radix Aucklandia were identified by TLC, and costuslactone content in Radix Aucklandia was determined by HPLC. RESULTS: The TLC identification was highly specific and spots were clear. Costuslactone in Radix Aucklandia showed a good linear relationship. The average recovery was 99.1% (RSD=1.2% and n=5). CONCLUSION: The methods are simple, reliable and have a good reproducibility and can be used for the quality control of Gujing Tablets. |
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| Keywords: | TLC HPLC |
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