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| 空心莲子草的化学成分研究 | |
| 引用本文： | 方进波,段宏泉,张彦文,高石喜久.空心莲子草的化学成分研究[J].中国中药杂志,2006,31(13):1072-1075. |
| 作者姓名： | 方进波 段宏泉 张彦文 高石喜久 |
| 作者单位： | 1. 天津大学,药学院,天津,300072 2. 天津医科大学,药学院,天津,300070 3. 日本国立德岛大学,药学部,日本,德岛,770-8505 |
| 摘 要： | 目的：分离空心莲子草Alternanthera philoxeroides的化学成分。方法：以硅胶柱、凝胶柱色谱分离,制备HPLC纯化,采用MS,NMR等波谱方法进行结构鉴定。结果：从石油醚及醋酸乙酯部位分离得到9个化合物：脱镁叶绿素a(phaeophytin a,1),脱镁叶绿素a′(pheophytin a′,2),齐墩果酸(oleanoic acid,3),β-谷甾醇(β-sitosterol,4),3β-羟基-豆甾-5-烯-7-酮(3β-hydroxystigmast-5-en-7-one,5),α-菠甾醇(α-spinasterol,6),二十四亚甲基环阿尔廷醇(24-methylenecycloartanol,7),环桉烯醇(cycloeucalenol,8),叶绿醇(phytol,9)。结论：化合物1,2,5,7～9均首次从该植物中分得。 |
| 关 键 词： | 空心莲子草 二十四亚甲基环阿尔廷醇 环桉烯醇 |
| 文章编号： | 1001-5302（2006）13-1072-04 |
| 收稿时间： | 2005-09-20 |
| 修稿时间： | 2005-09-20 |
Chemical constituents from herb of Alternanthera philoxeroides |
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| FANG Jin-bo ;DUAN Hong-quan ;ZHANG Yan-wen ;Yoshihisa Takaishi.Chemical constituents from herb of Alternanthera philoxeroides[J].China Journal of Chinese Materia Medica,2006,31(13):1072-1075. | |
| Authors: | FANG Jin-bo ;DUAN Hong-quan ;ZHANG Yan-wen ;Yoshihisa Takaishi |
| Institution: | 1. College of Pharmaceuticals, Tianjin University, Tianjin 300072, China; 2. Schod of Pharmacy, Tianjin Medical University, Tianjin 300070, China; 3. Faculty of Pharmaceutical Sciences,University of Tokushima,Tokushima 770-8505,Japan |
| Abstract: | OBJECTIVE: To study the active constituents from Alternanthera philoxeroides. METHOD: The constituents were isolated with silica gel and Toyopearl HW-40C gel column chromatography and purified by HPLC. Their structures were elucidated by spectroscopy. RESULT: Nine compounds were isolated and identified as phaeophytin a (1), pheophytin a' (2), oleanoic acid (3), beta-sitosterol (4), 3beta-hydroxystigmast-5-en-7-one (5), alpha-spinasterol (6), 24-methylenecycloartanol (7), cycloeucalenol (8), phytol (9). CONCLUSION: Compounds 1,2,5,7-9 were isolated from this plant for the first time. |
| Keywords: | Alternanthera philoxeroides 24-methylenecycloartanol cycloeucalenol |
| 本文献已被 CNKI 维普 万方数据 等数据库收录！ | |