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薄层扫描法测定祛腐生肌散中血竭素含量
引用本文:苑相爱. 薄层扫描法测定祛腐生肌散中血竭素含量[J]. 中国药业, 2010, 19(7): 17-18
作者姓名:苑相爱
作者单位:山东省安丘市中医院,山东,潍坊,262100
摘    要:目的建立医院自制制剂祛腐生肌散的质量控制方法。方法采用双波长反射法锯齿形薄层扫描法(λs=475nm)测定祛腐生肌散中血竭素含量。结果血竭素点样量在0.21—1.05μg范围内与吸光度呈良好的线性关系(r=0.9992),平均回收率为98.59%(RSD=0.94%)。结论所用方法简便、可靠、重现性好,可用于祛腐生肌散的质量控制。

关 键 词:祛腐生肌散  薄层扫描  血竭素  质量标准

Determination of Dracorhodin Content in Qufushengji Powder by TLC Scanning
Yuan Xiang'ai. Determination of Dracorhodin Content in Qufushengji Powder by TLC Scanning[J]. China Pharmaceuticals, 2010, 19(7): 17-18
Authors:Yuan Xiang'ai
Affiliation:Yuan Xiang' ai ( Anqiu Hospital of Traditional Chinese Medicine, Weifang, Shandong, China 262100)
Abstract:Objective To establish a quality standard for Qufushengji Powder. Methods Dual-wavelength reflection zigzag TLC scanning method was used to study the determination of dracorhodin in Qufushengji Powder (λs =475 nm). Results The good linear relationship was showed within the range of 0. 21 - 1.05 μg( r = 0. 999 2) for dracorhodin, and the average recovery rate was 98.59% ( RSD = 0. 94% ). Conclusion The established method is simple, accurate and reliable with good reproducibility, which can be used for the quality control of Qufushengji Powder..
Keywords:Qufushengji Powder  TLC scanning  dracorhodin  quality standard
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