| 牡丹皮免煎颗粒与饮片有效成分含量的差异研究 |
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| 引用本文： | 王晓琳,张平,郭敏.牡丹皮免煎颗粒与饮片有效成分含量的差异研究[J].甘肃中医,2010,23(12):43-44. |
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| 作者姓名： | 王晓琳 张平 郭敏 |
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| 作者单位： | 1. 甘肃省中医院,甘肃,兰州,730050
2. 甘肃省药品检验所 |
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| 摘 要： | 目的:比较中药牡丹皮免煎颗粒与其饮片中有效成分含量差异。方法:采用高效液相色谱法(HPLC),伊利特C18柱,以甲醇-水(50:50)为流动相,流速1.0 mL/min,检测波长274 nm。结果:牡丹皮免煎颗粒中丹皮酚含量为4.65 mg/g,牡丹皮中药饮片中丹皮酚含量为24.23 mg/g;丹皮酚在55～275μg范围内呈良好的线性关系,平均回收率为97.10%,RSD为0.7%(n=6)。结论:中药牡丹皮免煎颗粒与其饮片所含丹皮酚含量差异较大。
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| 关 键 词： | 免煎颗粒 丹皮酚 高效液相色谱法 |
Study of Effective Content of Paeonia Compared Fried Free Particles and Pieces |
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| WANG Xiao-ling,ZHANG Ping,GUO Min.Study of Effective Content of Paeonia Compared Fried Free Particles and Pieces[J].Gansu Journal of Traditional Chinese Medicine,2010,23(12):43-44. |
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| Authors: | WANG Xiao-ling ZHANG Ping GUO Min |
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| Institution: | 1 Gansu Province Hospital of TCM,Lanzhou Gansu China 730050 2 Gansu Institute for Drug Control ) |
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| Abstract: | Objective：To compare the difference of effective component paeonia between fried free particles and its pieces.Methods：To test with high performance liquid chromatography（HPLC）,Erie C18 column,with methanol-water（50：50） as mobile phase,velocity：1.0 mL/min,wavelength：274.Results：The content of polyphenol was 4.65 mg/g in fried free particles,24.23 mg/g in pieces.The polyphenol was linear relationship in range 55～275 μg,the average recovery was 97.10%,RSD for 0.7%,respectively.Conclusion： It was remarkable difference of content of polyphenol between fried free particles and its pieces. |
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| Keywords: | fried free particles polyphenol high performance liquid chromatography |
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