| 对中国药典用1-甲基海因鉴别哈蟆油方法的商榷 |
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| 引用本文： | 高竹青,刘俊亭,王春媛,高利娜,舒翠霞,牛晓东,祝娟,宋洋. 对中国药典用1-甲基海因鉴别哈蟆油方法的商榷[J]. 中南药学, 2013, 0(8): 608-610 |
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| 作者姓名： | 高竹青 刘俊亭 王春媛 高利娜 舒翠霞 牛晓东 祝娟 宋洋 |
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| 作者单位： | 中国医科大学药学院药物分析教研室,沈阳110001 |
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| 摘 要： | 目的检测哈蟆油及林蛙各组织中1-甲基海因（1-methylhydantoin,1-MID）。方法采用GC-MS法测定哈蟆油及林蛙各组织中1-MID。结果哈蟆油及林蛙其他组织均可检出1-MID。结论建立了哈蟆油中1-MID测定的方法;在林蛙的有关组织中均检测到含量不等的1-MID,用1-MID作为哈蟆油真伪鉴别的专属性有待研究。
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| 关 键 词： | 哈蟆油 1-甲基海因 林蛙 |
Query about 1-MID in the identification of Ranae oviducts in Chinese Pharmacopoeia |
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| GAO Zhu-qing,LIU Jun-ting,WANG Chun-yuan,GAO Li-na,SHU Cui-xia,NIU Xiao-dong,ZHU Juan,SONG Yang. Query about 1-MID in the identification of Ranae oviducts in Chinese Pharmacopoeia[J]. Central South Pharmacy, 2013, 0(8): 608-610 |
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| Authors: | GAO Zhu-qing LIU Jun-ting WANG Chun-yuan GAO Li-na SHU Cui-xia NIU Xiao-dong ZHU Juan SONG Yang |
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| Affiliation: | (Department of Pharmaceutical Analysis,China Medical University,Shenyang 110001) |
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| Abstract: | Objective To determine 1-methylhydantoin（1-MID） in Ranae oviducts and other tissues of rana.Methods GCMS was used to determine the 1-MID in the tissues of rana.Results We detected 1-MID in all samples.Conclusion A new method of assaying 1-MID in Ranae oviducts has been developed.According to this experiment,1-MID is detected with varying concentrations in the releted tissues of rana.The specification of 1-MID as the identification mark of Ranae oviducts in Chinese Pharmacopoeia 2010 should be further validated. |
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| Keywords: | Ranae oviducts 1-methylhydantoin rana |
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