| 不同产地柿蒂药材中没食子酸含量的比较 |
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| 引用本文： | 黄文平,;黄陆强,;宋永贵,;肖光清,;黎田儿,;李志峰.不同产地柿蒂药材中没食子酸含量的比较[J].江西中医学院学报,2014(3):58-59. |
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| 作者姓名： | 黄文平 ;黄陆强 ;宋永贵 ;肖光清 ;黎田儿 ;李志峰 |
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| 作者单位： | [1]中药固体制剂制造技术国家工程研究中心,江西南昌330006; [2]江西中医药大学,江西南昌330004 |
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| 摘 要： | 目的：采用RP-HPLC测定不同产地柿蒂药材中没食子酸的含量。方法：采用色谱柱：Cosmosil C18（4.6mm×250mm,5μm）,以甲醇-0.5%磷酸水溶液（5∶95）作流动相,流速：1.0mL/min;检测波长：273nm;柱温：25℃。结果：不同产地柿蒂中没食子酸含量在0.0177-0.1000%。结论：该方法简便、快速、准确可靠,不同产地柿蒂中没食子酸含量有较大的差异,其中以吉安新兴药材行（130801）的含量最高。
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| 关 键 词： | 柿蒂 没食子酸 高效液相色谱法 |
Comparing the Determination of Gallic Acid in Diospyros Kaki Thunb.from Different Areas |
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| Institution: | HUANG Wen - ping, HUANG Lu - qiang, SONG Yong - gui , XIAO Guang - qing, LI Tian - er, LI Zhi - feng(1. Solid Preparation of Traditional Chinese Medicine Manufacturing Technology National Engineering Center, Jiangxi, Nanehang 330006; 2. Jiangxi University of Traditional Chinese Medicine,Jiangxi, Nanchang 330004.) |
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| Abstract: | Objective：To establish an RP- HPLC determination of Gallic acid in Diospyros kaki Thunb from different sources.Methods：Cosmosil C18（4.6mm × 250mm,5μm）,methanol-0.5 % phosphoric acid solution（5∶95） as the mobile phase;flow rate：1.0 mL /min;detection wavelength：273nm;column temperature：25 ℃.Results：The content of Gallic acid was in 0.0177 - 0.1000% of Diospyros kaki Thunb.from different areas.Conclusion：The method is simple,rapid,accurate and Diospyros kaki Thunb.from different areas of Gallic acid has a bigger difference,with the highest content of Ji,an（130801）. |
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| Keywords: | iospyros kaki Gallic acid monohydrate HPLC |
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