| 稳心胶囊的制备及质量标准 |
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| 引用本文： | 陈海霞,李菁.稳心胶囊的制备及质量标准[J].山东大学学报(医学版),2009,47(7):136-140. |
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| 作者姓名： | 陈海霞 李菁 |
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| 作者单位： | 1. 山东大学齐鲁医院药剂科, 济南 250012； 2. 山东省职业卫生与职业病防治研究院药剂科, 济南 250002 |
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| 摘 要： | 目的建立稳心胶囊的制备方法及质量标准。方法采用薄层色谱法对处方中甘松、党参、三七进行定性鉴别；用高效液相色谱法测定制剂中人参皂苷Rg1和三七皂苷R1的含量。结果薄层色谱法专属性强；人参皂苷Rg1平均回收率为96.07%，RSD为0.33%；三七皂苷R1平均回收率为95.98%，RSD为0.56%。结论高效液相色谱法简便、准确，重复性好，可用于稳心胶囊的质量控制。
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| 关 键 词： | 稳心胶囊 色谱法，薄层 色谱法，高效液相 制备 质量标准 |
| 收稿时间： | 2008-07-17 |
Preparation of the Wenxin capsule and its quality standard |
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| CHEN Hai-xia,LI Jing.Preparation of the Wenxin capsule and its quality standard[J].Journal of Shandong University:Health Sciences,2009,47(7):136-140. |
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| Authors: | CHEN Hai-xia LI Jing |
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| Institution: | 1． Department of Pharmacy， Qilu Hospital of Shandong University, Jinan 250012, China;
2. Department of Pharmacy, Shandong Academy of Occupational Health and Occupational Medicine, Jinan 250002, China |
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| Abstract: | Objective To establish a preparation method and quality standard for the Wenxin capsule.Methods Thin-layer chromatography(TLC) was employed to identify Radix et Rhizoma Nardostachyos,Radix Codonopsis and Radix et Rhizoma Notoginseng.The contents of Ginsenoside Rg1 and Notoginsenoside R1 were determined by high pressure liquid chromatography.Results Quality control showed that identification by TLC was distinct and highly specific.The average recovery of Ginsenoside Rg1 was 96.07% with RSD at 0.33% and Notog... |
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| Keywords: | Wenxin capsules Chromatography thin-layer high pressure liquid Preparation Quality standard |
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