| HPLC法测定生发丸中二苯乙烯苷的含量 |
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| 引用本文： | 侯玉华,周小琴,丛晓东,孔艳.HPLC法测定生发丸中二苯乙烯苷的含量[J].中国药房,2010(36):3440-3442. |
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| 作者姓名： | 侯玉华 周小琴 丛晓东 孔艳 |
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| 作者单位： | [1]江苏徐州医药高等职业学校,徐州市221116 [2]浙江中医药大学,杭州市310053 [3]江苏徐州市中医院制剂室,徐州市221000 |
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| 摘 要： | 目的:建立以高效液相色谱法测定生发丸中二苯乙烯苷含量的方法。方法:色谱柱为SHMADZU shim-pack-vp-ODS(果150:二m苯m×乙4.烯6苷mm进,5样μ量m在)0,.柱21温～为1.2255μ℃g(,r流=动0.9相99为3乙)腈范-围水内(25线∶7性5关),系流良速好为1;.0回m收L率.m为i n9-61.4,4检%测,波RS长D为=32.270 n%m(n,=进6样)。量结为2论0:μ本L法。结简便、灵敏、专属性强,可用于生发丸中二苯乙烯苷的含量测定。
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| 关 键 词： | 生发丸 二苯乙烯苷 高效液相色谱法 |
Content of Stilbene Glucoside in Shengfa Pills by HPLC |
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| HOU Yu-hua,ZHOU Xiao-qinJiangsu Provincial Xuzhou Pharmaceutical Vocational College,Xuzhou,ChinaCONG Xiao-dongZhejiang University of TCM,Hangzhou,ChinaKONG Yan.Content of Stilbene Glucoside in Shengfa Pills by HPLC[J].China Pharmacy,2010(36):3440-3442. |
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| Authors: | HOU Yu-hua ZHOU Xiao-qinJiangsu Provincial Xuzhou Pharmaceutical Vocational College Xuzhou ChinaCONG Xiao-dongZhejiang University of TCM Hangzhou ChinaKONG Yan |
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| Institution: | HOU Yu-hua,ZHOU Xiao-qin(Jiangsu Provincial Xuzhou Pharmaceutical Vocational College,Xuzhou 221116,China)CONG Xiao-dong(Zhejiang University of TCM,Hangzhou 310053,China)KONG Yan(Preparation Room,Xuzhou Hospital of TCM,Xuzhou 221000,China) |
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| Abstract: | OBJECTIVE： To determinate the content of stilbene glucoside in Shengfa pills by HPLC.METHODS： SHMADZU shimpackvpODS（150 mm×4.6 mm,5 μm） column was adopted with acetonitrilewater（25 ∶ 75） as mobile phase at flow rate of 1.0 mL·min1.The detection wavelength was set at 320 nm and injection volume was 20 μL.RESULTS： The linear range of stilbene glucoside was 0.21～1.25 μg（r=0.999 3） with recovery of 96.44%（RSD=2.7%,n=6）.CONCLUSION： The method is simple,sensitive and specific for the content determination of stilbene glucoside in Shengfa pills. |
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| Keywords: | Shengfa pills Stilbene glucoside HPLC |
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