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泰山紫草和新疆紫草挥发油成分的GC-MS分析
引用本文:谷红霞,冀海伟,翟静. 泰山紫草和新疆紫草挥发油成分的GC-MS分析[J]. 中国药房, 2010, 0(27): 2546-2548
作者姓名:谷红霞  冀海伟  翟静
作者单位:[1]山东泰安市中心医院中药房,泰安市271000 [2]泰山医学院化学与化学工程学院,泰安市271016 [3]泰山医学院基础医学部,泰安市271000
基金项目:山东省中医药科技发展计划项目(2007-167)
摘    要:目的:分析比较泰山紫草与新疆紫草干燥根的挥发油成分。方法:用水蒸气蒸馏法提取泰山紫草与新疆紫草干燥根挥发油,用气相色谱-质谱(GC-MS)联用法进行分析测定。结果:从泰山紫草与新疆紫草干燥根挥发油中分别鉴定出34种和36种成分,占挥发油色谱总峰面积的70.16%和74.79%,其中共有组分为4种。泰山紫草挥发油中相对质量分数较高的组分为2,6-二叔丁基对甲酚(9.29%)、2,4-二叔丁基-1,3戊二烯(8.17%)和反式橙花叔醇(6.05%);新疆紫草中相对质量分数较高的组分为诱虫烯(16.28%)、3-烯丙基-2-甲氧基苯酚(6.20%)与樟脑(5.82%)。结论:本试验可为紫草的进一步开发和利用提供科学根据。

关 键 词:泰山紫草  新疆紫草  挥发油  化学成分  气相色谱-质谱联用法

Analysis of the Volatile Oil from Lithospermum erythrorhizon and Arnebia euchroma by GC-MS
GU Hong-xia,JI Hai-wei,ZHAI Jing. Analysis of the Volatile Oil from Lithospermum erythrorhizon and Arnebia euchroma by GC-MS[J]. China Pharmacy, 2010, 0(27): 2546-2548
Authors:GU Hong-xia  JI Hai-wei  ZHAI Jing
Affiliation:1Dept.of TCM Pharmacy,Tai'an Municipal Central Hospital of Shandong Province,Tai'an 271000,China;2College of Chemistry and Chemical Engineering,Taishan Medical University,Tai'an 271016,China;3Dept.of Basic Medicine,Taishan Medical University,Tai'an 271000,China)
Abstract:OBJECTIVE:To analyze the volatile oil extracted from the root of Lithospermum erythrorhizon and Arnebia euchroma.METHODS:Volatile oil were extracted from L.erythrorhizon and A.euchroma by steam distillation and determined by GC-MS.RESULTS:34 components and 36 components of volatile oil extracted from the root of L.erythrorhizon and A.euchroma were separated and identified respectively,accounting for 70.16% and 74.79% of the total peak area.There were 4 kinds of common peak among these components.The main components were 2,6-di-tert-butyl-p-Cresol(9.29%),2,4-di-t-butyl-1,3-Pentadiene(8.17%),and trans-Nerolidol(6.05%) in L.erythrorhizon and muscalure(16.28%),3-Allyl-2-methoxyphenol(6.20%)and camphor(5.82%) in A.euchroma.CONCLUSION:The study can provide scientific basis for the further development of Radix Arnebiae.
Keywords:Lithospermum erythorhizon  Arnebia euchroma  Volatile oil  Chemical components  GC-MS.
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