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市售生、煅炉甘石的成分分析及质量评价
引用本文:周灵君,张丽,路长珍,丁安伟.市售生、煅炉甘石的成分分析及质量评价[J].中国药房,2010(27):2534-2536.
作者姓名:周灵君  张丽  路长珍  丁安伟
作者单位:南京中医药大学药学院/江苏省方剂研究重点实验室,南京市210046
基金项目:2010年版《中国药典》(一部)标准研究课题(YS-129); 江苏省普通高校研究生科研创新计划资助项目(CX09B_2802)
摘    要:目的:对市售矿物药生、煅炉甘石进行成分分析和质量评价。方法:采用X射线衍射(XRD)法对17批生炉甘石和13批煅炉甘石样品进行成分分析,并按2005年版《中国药典》规定方法测定ZnO含量。结果:市售生、煅炉甘石XRD谱显示其多为CaCO3及其它杂质而无应有的ZnCO3或ZnO。结论:XRD法可以应用于矿物药生、煅炉甘石的鉴定及其质量控制。

关 键 词:X射线衍射法  炉甘石  煅炉甘石  矿物药  质量

Component Analysis and Quality Evaluation of Original and Calcined Calamine for Sale
ZHOU Ling-jun,ZHANG Li,LU Chang-zhen,DING An-wei.Component Analysis and Quality Evaluation of Original and Calcined Calamine for Sale[J].China Pharmacy,2010(27):2534-2536.
Authors:ZHOU Ling-jun  ZHANG Li  LU Chang-zhen  DING An-wei
Institution:(College of Pharmacy,Nanjing University of Traditional Chinese Medicine,Jiangsu Key Laboratory for TCM Formula Research,Nanjing 210046,China)
Abstract:OBJECTIVE:To analyze the component of original and calcined calamine for sale,and to evaluate its quality.METHODS:X-ray powder diffraction(XRD) was used to analyze the components of 17 batches of original calamine and 13 batches of calcined calamine.The content of ZnO was determined according to Chinese Pharmacopeia(2005 edition).RESULTS:The XRD spectrum of original and calcined calamine showed that most of them were CaCO3 and other impurities but not ZnCO3 or ZnO.CONCLUSION:XRD can be applied for the identification of quality control of original and calcined calamine.
Keywords:X-ray powder diffraction  Calamine  Calcined calamine  Mineral drugs  Quality
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