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鲜地黄的闪式提取工艺优选
引用本文:张庆岭.鲜地黄的闪式提取工艺优选[J].中国实验方剂学杂志,2013,19(1):62-63.
作者姓名:张庆岭
作者单位:焦作卫生医药学校,河南焦作,454001
摘    要:目的:优选鲜地黄的闪式提取工艺。方法:以梓醇及干膏得量为评价指标,选取提取时间、提取次数及溶剂用量为考察因素,通过单因素试验及正交试验优选闪式提取工艺。采用RP-HPLC测定指标成分含量。结果:最佳闪式提取工艺为加3倍量95%乙醇提取1次,提取时间3 min。结论:优选的工艺快速、合理。

关 键 词:鲜地黄  闪式提取  正交试验  梓醇  干膏得量
收稿时间:2012/7/23 0:00:00

Optimization of Flash Extraction Technology for Fresh Rehmannia glutinosa
ZHANG Qing-ling.Optimization of Flash Extraction Technology for Fresh Rehmannia glutinosa[J].China Journal of Experimental Traditional Medical Formulae,2013,19(1):62-63.
Authors:ZHANG Qing-ling
Institution:Jiaozuo Medical and Health School, Jiaozuo 454001, China
Abstract:Objective:To optimize flash extraction technology of fresh Rehmannia glutinosa. Method: With catalpol and yield of dry extract as indexes,extraction time,extraction times and solvent consumption were chosen as factors,flash extraction technology of fresh R. glutinosa was optimized by orthogonal test and single factor test.The content of indicator ingredients was determined by HPLC. Result: Optimum flash extraction process was:extrated 1 times with 3 times the amount of 95% ethanol,extraction time of 3 minutes. Conclusion: This optimized process was fast,scientific and reasonable.
Keywords:fresh Rehmannia glutinosa  flash extraction  orthogonal test  catalpol  yield of dry extract
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