舒痔丸质量标准研究

目的：提高舒痔丸的质量标准。方法：采用TLC法对舒痔丸中黄芩、大黄、当归、牡丹皮进行定性鉴别；用HPLC法对舒痔丸中黄芩苷、丹皮酚进行含量测定。结果：在TLC色谱中均能检出黄芩、大黄、当归，牡丹皮；黄芩苷进样量在0．0768-0．6400μg范围内呈良好的线性关系（r=0．9999），平均回收率为99．4％，RSD为0．32％；丹皮酚进样量在0．04168-0．4168μg范围内呈良好的线性关系（r=0．9997），平均回收率为99．0％，RSD为0．53％。结论：所建立的方法快捷，重现性好，专属性强，可用于舒痔丸的质量控制。

Quality Standards for Shuzhi Pills

Objective：To establish the quality standards for Shuzhi pills. Method： Scutellariae Radix, Rhei Radix et Rhizoma,Angelicae Sinesnsis Radix, Cortex Mutan in Shuzhi Pills were identified by TLC, and baicalin and paeconol were determined by HPLC. Result： Scutellariae Radix, Rhei Radix et Rhizoma, Angelicae Sinesnsis Radix, Cortex Mutan could be detected by TLC. The linear range of baicalin was 0. 076 8 - 0. 640 0 μg （ r = 0. 999 9）. The average recovery was 99.4% , and RSD was 0. 32%. The linear range of paeconol was 0. 041 68 -0. 416 8 μg. （r =0. 999 7）. The average recovery was 99.0% , and RSD was 0. 53 %. Conciusion： The method is fast with good reproducibility and high specific. It can be used for the quality control of Shuzhi Pills.