| 香芍疏肝口服液质量标准研究 |
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| 引用本文： | 毕晓黎,彭丽诗,李素梅.香芍疏肝口服液质量标准研究[J].江西中医学院学报,2014,0(2):61-64. |
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| 作者姓名： | 毕晓黎 彭丽诗 李素梅 |
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| 作者单位： | 毕晓黎 (广东省中医药工程技术研究院 广东 广州510095 广州中医药大学 广东广州510405)； 彭丽诗 (广州中医药大学 广东广州510405)； 李素梅(广东省中医药工程技术研究院 广东 广州510095)； |
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| 摘 要： | 目的：建立香芍疏肝口服液的质量控制标准。方法：采用薄层色谱法对制剂中的香附、白芍和柴胡进行定性鉴别；采，高效液相色谱法对制剂中的芍药苷进行含量测定。结果：薄层色谱法可鉴别出香附、白芍和柴胡，斑点清晰，分离度好，且E性对照无干扰；芍药苷在0．2308—1．1540μg范围内呈良好线性关系，r=0．9999，平均回收率为98．05％，RSD=0．91％。结论本方法操作简便易行、准确可靠、灵敏度高、重现性好，可作为香芍疏肝口服液的质量控制方法。
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| 关 键 词： | 香芍疏肝口服液 薄层色谱法 高效液相色谱法 芍药苷 质量标准 |
Study on the Quality Standard of Xiangshao Shugan Oral Liquid |
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| Institution: | BI Xiao - li, PENG Li - shi, LI Su - mei( 1. Guangdong Province Engineering Technology Research Institute of Traditional Chinese Medicine, Guangzhou 510095, China ; 2. Guangzhou University of Chinese Medicine, Gnangzhou 510405, China.) |
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| Abstract: | Objective： To establish the quality standard of Xiangshao Shugan Oral Liquid. Methods： Rhizoma Cyperi, Radix Paeoniae Alba and Radix Bupleuri in Xiangshao Shugan Oral Liquid were identified by TLC. The content of Paeoniflorin was determined by HPLC. Results ： The TLC spots of Rhizoma Cyperi, Radix Paeoniae Alba and Radix Bupleuri were clear with good separation and free of interference of negative samples. The linear ranges of Paeoniflorin was 0. 2308 - 1. 1540μg, the average recovery rate was 98.05% , RSD = 0.91%. Conclusion ： The method is simple, accurate, sensitive and reliable, which can be used to control the quality of Xiangsbao Shugan Oral Liquid. |
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| Keywords: | Xiangshao Shugan Oral Liquid TLC HPLC Paeoniflorin quality standard |
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