| 小儿清热止咳颗粒剂质量标准研究 |
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| 引用本文： | 钟瑞建,叶久之,张峰.小儿清热止咳颗粒剂质量标准研究[J].中国药品标准,2001,2(4):62-64. |
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| 作者姓名： | 钟瑞建 叶久之 张峰 |
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| 作者单位： | 1. 江西省药品检验所,南昌,330046
2. 太极集团·浙江东方制药有限公司,绍兴,312000 |
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| 摘 要： | 目的：制订小儿清热止咳颗粒剂质量标准。方法：对杏仁药材进行了薄层色谱鉴别，紫外分光光度法测定了总黄酮的含量，结果：回收率为98．45％（RSD％＝1．83％，n=6)，线性范围为2．72ug/ml-19.04ug/ml，线性关系r=0.9998，重复线RSD＝1．09％（n=6)，精密度RSD＝0．91％（n=6)，结论：方法稳定，可靠，可作为该制剂的质量控制方法之一。
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| 关 键 词： | 总黄酮 含量测定 杏仁 薄层色谱鉴别 |
STUDY OF QUALITY STANDARD OF XIAO'ER QINGRE ZHIKE KELI |
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| Authors: | Zhong Ruijian Ye Jiuzhi and Zhang Feng |
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| Institution: | Jiangxi Institute for Drug Control, Nanchang 330046;Jiangxi Institute for Drug Control, Nanchang 330046;Zhejiang East Phaemaceutical Co. Ltd Of Taiji Group, Shaoxing 312000 |
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| Abstract: | Objective:To set down the quality standard of Xiao'er Qingre Zhike Keli. Methods:Determination of Flavone in Xiao'er Qingre Zhike Keli by UV. The Apricot was separated by TLC. Results:The average recovery is 98.45%(RSD=1. 83% ,n = 6) ,with good linear relationship(r = 0. 9998)and repetition (RSD=1. 09%,n = 6)and precision(RSD=0. 91%,n = 6) Conclusions:The method is accurate,reliable-It can be one of method for quality control of the production. |
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| Keywords: | flavone determining content apricot TLC |
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