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| 双黄安神颗粒质量标准研究 | |
| 引用本文： | 陈庆伟,翁一玲,朱国理. 双黄安神颗粒质量标准研究[J]. 海峡药学, 2012, 24(6): 44-46 |
| 作者姓名： | 陈庆伟 翁一玲 朱国理 |
| 作者单位： | 1. 福建省福州市药品检验所,福州,350007 2. 福建中医药大学附属第二人民医院,福州,350003 3. 福州长富星新药开发有限公司,福州,350002 |
| 摘 要： | 目的 建立双黄安神颗粒的质量标准.方法 对方中大黄建立TLC鉴别,用高效液相色谱法对盐酸麻黄碱进行测定.结果 盐酸麻黄碱在27.264～272.64ng范围内与峰面积呈良好的线性关系,平均加样回收率为98.8%.结论 该法操作简便,结果准确,重复性好,可以控制双黄安神颗粒的质量. |
| 关 键 词： | 双黄安神颗粒 质量标准 盐酸麻黄碱 HPLC |
Quality standard for Shuanghuang Anshen Granules |
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| CHEN Qing-wei , WENG Yi-ling , ZHU Guo-li. Quality standard for Shuanghuang Anshen Granules[J]. Strait Pharmaceutical Journal, 2012, 24(6): 44-46 | |
| Authors: | CHEN Qing-wei WENG Yi-ling ZHU Guo-li |
| Affiliation: | 1.Fuzhou Institute for Drug Control,Fuzhou 350007,China;2.Second Affiliated People’s Hospital of Fujian University of Chinese Medicine,Fuzhou 350003,China;3.Fuzhou Changfuxing Pharmaceutical Development Co,Ltd,Fuzhou 350002,China) |
| Abstract: | OBJECTIVE To establish the quality standard for Shuanghuang Anshen Granules.METHODS TLC was used to identify Radix et Rhizoma Rhei.The content of Ephedrine hydrochloride was determined by HPLC.RESULTS The linear range of Ephedrine hydrochloride was 27.264~272.64ng.The average recovery was 98.8%.CONCLUSION The method is simple.the result is accurate and the reproducibility is good and can be used as the quality control of Shuanghuang Anshen Granules. |
| Keywords: | Shuanghuang Anshen Granules Quality standard Ephedrine Hydrochloride HPLC |
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