| 气相色谱法检测一次性使用输液器中环己酮残留量 |
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| 引用本文： | 方彩飞. 气相色谱法检测一次性使用输液器中环己酮残留量[J]. 中国药师, 2014, 0(10): 1780-1781 |
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| 作者姓名： | 方彩飞 |
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| 作者单位： | 武汉市第一医院 武汉 430022 |
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| 摘 要： | 目的：建立气相色谱法检测一次性使用输液器中环己酮残留量的方法。方法：采用DB-FFAP（30 m ×0.32 mm,0.25μm）毛细管柱,以氮气为载气,FID检测,程序升温。结果：环己酮在0.01~0.50μg·ml-1范围内线性关系良好（ r=0.9991）,最低检测限为1 ng·ml^-1。结论：本方法简便、准确、快速,可用于一次性使用输液器中环己酮残留量的测定。
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| 关 键 词： | 环己酮 气相色谱法 顶空进样 一次性使用 输液器 |
| 收稿时间： | 2014-03-04 |
| 修稿时间： | 2014-06-17 |
Determination of Residual Cyclohexanone in Disposable Infusion Set by Gas Chromatography |
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| Fang Caifei. Determination of Residual Cyclohexanone in Disposable Infusion Set by Gas Chromatography[J]. China Pharmacist, 2014, 0(10): 1780-1781 |
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| Authors: | Fang Caifei |
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| Affiliation: | The First Hospital of Wuhan, Wuhan 430022, China |
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| Abstract: | Objective： To establish a determination method for residual cyclohexanone in the disposable infusion set by GC. Meth- ods： The capillary column was DB-FFAP （30 m ×0.32 mm,0, 25 μm）. The carrier gas was nitrogen and an FID was used as the de- tector. The column temperature was raised by program. Results： The calibration curve was linear within the range of 0.01-0.50 .g . ml - 1 （ r = 0. 999 1 ） and the detection limit was 1 ng .ml ^- 1. Conclusion： The method is simple, accurate and rapid, and suitable for the determination of residual cyclohexanone in the disposable infusion set. |
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| Keywords: | Cyclohexanone Gas chromatography Headspace injection Disposable infusion set |
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