| 景洪哥纳香的化学成分研究Ⅱ |
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| 引用本文： | 顾正兵,刘乃兵,徐一新,梁华清,陈海生,张卫东. 景洪哥纳香的化学成分研究Ⅱ[J]. 中国药学杂志, 2001, 36(6): 376-378 |
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| 作者姓名： | 顾正兵 刘乃兵 徐一新 梁华清 陈海生 张卫东 |
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| 作者单位： | 1. 第二军医大学药学院,
2. 解放军55266部队业务处, |
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| 摘 要： | 目的分离鉴定景洪哥纳香化学成分。方法用乙醇提取、硅胶柱层析分离，通过IR，NMR及MS光谱分析法确定结构。结果分得5个化合物，分别鉴定为8-羟基-7-苯基-2，6-二氧双环［3，3，1］壬烷-3-酮(Ⅰ)、10-氨基-4-羧基-3，8-二甲氧基菲-1-羧酸内酰胺(Ⅱ)、10-氨基4，8-二羟基-3-甲氧基菲-1-羧酸内酰胺(Ⅲ)、β-谷甾醇(Ⅳ)和β-胡萝卜苷（Ⅴ)。结论分得的5个化合物均为首次从该植物中发现，化合物Ⅲ为新化合物。
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| 关 键 词： | 景洪哥纳香 菲内酰胺生物碱 10-氨基-4 8-二羟基-3-甲氧基菲-1-羧酸内酰胺 |
| 文章编号： | 1001-2494(2001)06-0376-03 |
| 收稿时间： | 2000-09-21; |
| 修稿时间： | 2000-09-21 |
Chemical constituents of Goniothalamus cheliensis |
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| GU Zheng bing ,LIU Nai bing ,XU Yi xin ,Liang Hua qing ,CHEN Hai sheng ,ZHANG Wei dong. Chemical constituents of Goniothalamus cheliensis[J]. Chinese Pharmaceutical Journal, 2001, 36(6): 376-378 |
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| Authors: | GU Zheng bing LIU Nai bing XU Yi xin Liang Hua qing CHEN Hai sheng ZHANG Wei dong |
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| Affiliation: | GU Zheng bing 1,LIU Nai bing 2,XU Yi xin 1,Liang Hua qing 1,CHEN Hai sheng 1,ZHANG Wei dong 1 |
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| Abstract: | OBJECTIVE To islate and elucidate the constituents of Goniothalamus cheliensis.METHODS The compounds were extracted by 95% alcohol and isolated by chromatography on silica gel.Their structures were determined by IR,1H-NMR,13C-NMR and MS spectra respectively.RESULTS Five compounds were elucidated as 8-hydroxy-7-phenyl-2,6-dioxybicyclo［3,3,1］nonan-3-one,10-amino 3,8-dimethoxy-4-hydroxyphenanthrene-1-carboxylic acid lactam,10-amino-4,8-dihydroxy-3 methoxyphenanthrene-1-carboxylic acid lactam,β-sitosterol and β-sitosterol-3-O-β-D glucopyranoside. CONCLUSION All compounds were separated from the bark of Goniothalamus cheliensis Hu.for the first time.Among them,Ⅲ is a new compound. |
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| Keywords: | Goniothalamus cheliensis phenanthrene lactam 10 amino 4 8 dihydroxy 3 methoxyphenanthrene 1 carboxylic acid lactam |
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