| HS-SPME-GC-MS分析香荚兰豆中挥发性成分 |
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| 引用本文： | 卢金清,李雨玲,张锐,杨小金,郭彧,江汉美,李肖爽.HS-SPME-GC-MS分析香荚兰豆中挥发性成分[J].中国实验方剂学杂志,2014,20(3):79-82. |
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| 作者姓名： | 卢金清 李雨玲 张锐 杨小金 郭彧 江汉美 李肖爽 |
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| 作者单位： | 湖北中医药大学/湖北省药用植物研发中心, 武汉 430065;湖北中医药大学/湖北省药用植物研发中心, 武汉 430065;湖北中医药大学/湖北省药用植物研发中心, 武汉 430065;湖北中医药大学/湖北省药用植物研发中心, 武汉 430065;湖北中医药大学/湖北省药用植物研发中心, 武汉 430065;湖北中医药大学/湖北省药用植物研发中心, 武汉 430065;湖北中医药大学/湖北省药用植物研发中心, 武汉 430065 |
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| 基金项目： | 湖北省自然科学基金项目（2004AB242） |
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| 摘 要： | 目的： 研究香荚兰豆中挥发性成分的化学组成。 方法： 采用顶空固相微萃取（HS-SPME）技术对香荚兰豆挥发性成分进行萃取、富集，气相色谱-质谱（GC-MS）法进行分离分析，并筛选了固相微萃取纤维头，优化了SPME的操作条件。 结果： 共分离并鉴定出28种化学成分，占挥发性成分总量的98.17%。香荚兰豆挥发性成分中含量最高的是香兰素（48.28%），其次为愈创木酚（15.54%）。 结论： 采用HS-SPME-GC-MS联用技术分析香荚兰豆挥发性成分，为香荚兰豆进一步研究及综合开发利用提供科学依据。
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| 关 键 词： | 香荚兰豆 固相微萃取 气相色谱-质谱 挥发性成分 |
| 收稿时间： | 2013/5/24 0:00:00 |
Analysis of Volatile Chemical Constituents in Vanilla planifoli by HS-SPME-GC-MS |
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| LU Jin-qing,LI Yu-ling,ZHANG Rui,YANG Xiao-jin,GUO Yu,JIANG Han-mei and LI Xiao-shuang.Analysis of Volatile Chemical Constituents in Vanilla planifoli by HS-SPME-GC-MS[J].China Journal of Experimental Traditional Medical Formulae,2014,20(3):79-82. |
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| Authors: | LU Jin-qing LI Yu-ling ZHANG Rui YANG Xiao-jin GUO Yu JIANG Han-mei and LI Xiao-shuang |
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| Institution: | Hubei University of Traditional Chinese Medicine/Research and Development Center of Medicinal Plants in Hubei Province, Wuhan 430065, China;Hubei University of Traditional Chinese Medicine/Research and Development Center of Medicinal Plants in Hubei Province, Wuhan 430065, China;Hubei University of Traditional Chinese Medicine/Research and Development Center of Medicinal Plants in Hubei Province, Wuhan 430065, China;Hubei University of Traditional Chinese Medicine/Research and Development Center of Medicinal Plants in Hubei Province, Wuhan 430065, China;Hubei University of Traditional Chinese Medicine/Research and Development Center of Medicinal Plants in Hubei Province, Wuhan 430065, China;Hubei University of Traditional Chinese Medicine/Research and Development Center of Medicinal Plants in Hubei Province, Wuhan 430065, China;Hubei University of Traditional Chinese Medicine/Research and Development Center of Medicinal Plants in Hubei Province, Wuhan 430065, China |
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| Abstract: | Objective: To analyze the volatile components from fruit of Vanill planifol. Method: The volatile chemical constituents were extracted and enriched by headspace solid phase micro-extraction (HS-SPME). The chemical components were analyzed by GC-MS. Selected the solid phase micro-extraction fiber head, while optimized the HS-SPME operating conditions. Result: A total of 28 components were separated and identified, accounted for 98.17% of total volatile components. The main component is vanillin (48.28%) and 2-methoxy-phenol (15.54%). Conclusion: This is the first time to adopt HS-SPME combined with GC-MS to analyze the volatile chemical components from fruit of V. planifoli and this study can provide scientific basis for further research and development of volatile chemical constituents of V. planifoli. |
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| Keywords: | Vanilla planifoli Andrews HS-SPME GC-MS volatile chemical constituents |
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