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混合酸消解-EDTA滴定法测定头发中钙
引用本文:过治勇,王丰舟.混合酸消解-EDTA滴定法测定头发中钙[J].河南预防医学杂志,2012,23(5):369-370.
作者姓名:过治勇  王丰舟
作者单位:尉氏县疾病预防控制中心,河南尉氏,475500
摘    要:目的建立EDTA滴定法测定头发中钙的方法。方法采用混合酸将头发消解后用去离子水定容,用EDTA标准滴定溶液滴定。结果滴定法测定头发中钙相对标准偏差为1.32%~2.61%,回收率为88.80%~110.40%。结论 EDTA滴定法测定头发中钙简便,精密度和准确度高,可作为测定头发中钙的方法。

关 键 词:消解  EDTA滴定法  头发  

Mixed acid digestion-EDTA titration determination of calcium in hair
GUO Zhi-yong , WANG Feng-zhou.Mixed acid digestion-EDTA titration determination of calcium in hair[J].Henan Journal of Preventive Medicine,2012,23(5):369-370.
Authors:GUO Zhi-yong  WANG Feng-zhou
Institution:.Weishi center for Disease Control and Prevention,Henan 475500 China.
Abstract:Objective To establish EDTA titration determination to determine the calcium in hair.Methods Use mixed acid digestion to digeste the hair,then bring to volume by deionized water,last use the method of EDTA titration determination to determine the calcium in hair.Results Dealing with the hair by mixed acid digestion,the relative standard deviation(RSD) of the method is 1.32 %~2.61 %,and recoveries is 88.80 %~110.40 %.Conclusion The method of mixed acid digestion-EDTA titration determination of calcium in hair is simple,Precition and Accuracy are fine.it can be used to determine the calcium in hair.
Keywords:mixed acid digestion  EDTA titration determination  hair  calcium
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