| 那如-3凝胶剂质量标准的研究 |
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| 引用本文： | 温爱平 苏瑞林. 那如-3凝胶剂质量标准的研究[J]. 药物分析杂志, 2005, 25(12): 1466-1468 |
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| 作者姓名： | 温爱平 苏瑞林 |
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| 作者单位： | [1]内蒙古医学院药学系,呼和浩特010059 [2]包头市药检所,包头014000 |
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| 摘 要： | 目的：建立那如-3凝胶剂的质量标准。方法：采用薄层色谱法对方中的草乌、诃子和荜茇进行鉴别。用高效液相色谱法对荜茇中有效成分胡椒碱进行含量测定。色谱柱为ZORBAX Eclipse XDB-C18柱；流动相为甲醇-水（77：23）；检测波长为343nm。结果：薄层鉴别色谱特征斑点明显，胡椒碱在0．1～0．8ug范围内呈良好的线性关系，平均回收率为100．5％（RSD=1．7％）。结论：本法能较好地控制那如-3凝胶剂的质量。
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| 关 键 词： | 那如-3凝胶剂 胡椒碱 TLC HPLC 质量标准 |
| 修稿时间： | 2005-04-13 |
Study on Quality Standard of Naru- 3 Gel |
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| Wen Ai - ping , Shu Rui - lin. Study on Quality Standard of Naru- 3 Gel[J]. Chinese Journal of Pharmaceutical Analysis, 2005, 25(12): 1466-1468 |
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| Authors: | Wen Ai - ping Shu Rui - lin |
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| Affiliation: | Department of pharmacy,Inner Mongolia medical college Huhhot 010059, China |
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| Abstract: | Objective:To establish a quality standard for Naru-3 Gel.Method:Aconitum Kusnezoffii Reichb,Ter- minalia Chebula Retz.And Piper longum L.were identified by TLC.The content of piperine in Naru-3 gel was de- termined by HPLC,using a ZORBAX Eclipse XDB-C_(18)column,methanol-water(77:23)as mobile phase;the detecting wavelength was 343 nm.Results:The TLC spots developed were quite clear,The linear range of piperine was 0.1 ug-0.8 ug,The average recovery of piperine was 100.5% with RSD of 1.7%.Conclusion:The method can be used to the quality control of Naru-3 Gel. |
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| Keywords: | Naru - 3 Gel piperine TLC HPLC |
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