| 宁神解郁胶囊质量标准研究 |
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| 引用本文： | 周洪合,张小平.宁神解郁胶囊质量标准研究[J].中国医疗前沿,2012(20):69-70. |
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| 作者姓名： | 周洪合 张小平 |
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| 作者单位： | 山东省济南市第三人民医院;济南市中医医院 |
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| 摘 要： | 目的建立宁神解郁胶囊的质量标准。方法采用TLC法对宁神解郁胶囊中黄芪、当归、白芍进行了定性鉴别;采用HPLC法测定芍药苷的含量,为宁神解郁胶囊的质量控制提供依据。结果定性鉴别方法专属性强;在6-30μg范围内芍药苷峰面积与进样量线性关系良好,r-0.9999;样品加样回收率为99.75%（n=5）。RSD为0.76。结论所建立的方法准确可行,重复性好,可有效控制宁神解郁胶囊的质量。
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| 关 键 词： | 宁神解郁胶囊 质量标准 芍药苷 高效液相色谱法 |
A Study ln the Qualigy Standard for Ningshenjieyu Capsules |
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| ZHOU Hong-he,ZHANG Xiao-ping.A Study ln the Qualigy Standard for Ningshenjieyu Capsules[J].China Healthcare Innovation,2012(20):69-70. |
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| Authors: | ZHOU Hong-he ZHANG Xiao-ping |
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| Institution: | .Third People’s Hospital of Jinan City,Jinan 250101,China |
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| Abstract: | Objictive To establish tile quality standard for Ningshenjieyu Capsules. Methods Thinlayer chromatogramphy（TLC） was used for qualitative klentifyication of Radix Astragali; Radix Angelicae Sinensis; The Paeontflorin was determined by HPLC. Remflts TLC identifyication was highly specific; The Paeonfflorin area and content showed a good linesr relationship ym the range of 6-30μg and correlateion coefficient was 0.9999. The average recorery of the added sample was 99.75%（n=5）, RSD was 0.76%. Conclusion The method is stable,accurate and precise for the quality control of Ningshenjieyu Capsules. |
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| Keywords: | Ningshenjieyu Capsules Quality standard Paeontflorin HPLC |
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