火焰原子吸收分光光度法测定乳酸钙片中乳酸钙含量 |
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引用本文: | 张新芹,周礼玲. 火焰原子吸收分光光度法测定乳酸钙片中乳酸钙含量[J]. 黑龙江医药, 2013, 0(6): 970-971 |
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作者姓名: | 张新芹 周礼玲 |
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作者单位: | 六安市食品药品检验所,237000 |
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摘 要: | 目的:测定乳酸钙片中乳酸钙的含量。方法:用水制备供试品溶液,加入氯化镧消除干扰,将供试品溶液喷入乙炔一空气火焰,用标准曲线法测定钙的含量。结果:钙元素在0~6.00μg/ml范围内,线性关系良好,相关系数r=0.9984;在标示量的80%、100%、120%三个浓度点测定回收率,平均回收率为99.6%,RSD为1.8%(n=9)。结论:本法简单、快速、准确、重现性好,适用于乳酸钙片中乳酸钙的含量测定。
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关 键 词: | 原子吸收分光光度法 乳酸钙片 |
Determination of Calcium Lacate in Compound Calcium Lactate Tablets by Flame Atomic Absorption Spectrometry |
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Affiliation: | Zhang Xinqin ,et al Luan Institute for Drug Control, Anhui(237000) |
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Abstract: | Objective:A flame atomic absorption spectrometry method for the determination of calcium lactate in Compound Calcium Lactate Tablets was established.Methods:The sample solutions were prepared with water and sodium chloride was added to eliminate ionization interference.Results:The sample solutions were injected into air-acetylene flame.The content of potassium were calculat-ed by standard calibration curves.The linear range fro potassium chloride was 0~6.00μg/ml,r=0.9984.The average recovery rate was 99.6%,RSD=1.8%(n=9).Conclusion:The method is simple,rapid,accurate and reproductive. |
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Keywords: | flame atomic absorption spectrometry Calcium Lactate Tablets |
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