| 运用HPLC法测定妇月康胶囊中阿魏酸的含量 |
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| 引用本文： | 蒋俊春,孟建升. 运用HPLC法测定妇月康胶囊中阿魏酸的含量[J]. 中国中医药现代远程教育, 2011, 9(14): 157-158. DOI: 10.3969/j.issn.1672-2779.2011.14.107 |
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| 作者姓名： | 蒋俊春 孟建升 |
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| 作者单位： | 河南省商丘市食品药品检验所,商丘,476000 |
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| 摘 要： | 目的建立HPLC法测定妇月康胶囊中阿魏酸含量的方法。方法采用EclipseXDB-C18色谱柱,甲醇:5%冰醋酸溶液(22:78)为流动相;流速1.0ml?min-1;检测波长322nm。结果阿魏酸在8.208～41.04μg?ml-1范围内线性关系良好(r=0.9999),平均回收率为99.07%,RSD=1.63%(n=6)。结论本方法操作简便,专属性强,结果准确,可用于妇月康胶囊的质量控制。
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| 关 键 词： | 高效液相色谱法 阿魏酸 含量测定 |
Determination of Ferulic Acid in Fuyuekang Capsules by HPLC |
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| Jiang Junchun,Meng Jiansheng. Determination of Ferulic Acid in Fuyuekang Capsules by HPLC[J]. Chinese Medicine Modern Distance Education of China, 2011, 9(14): 157-158. DOI: 10.3969/j.issn.1672-2779.2011.14.107 |
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| Authors: | Jiang Junchun Meng Jiansheng |
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| Affiliation: | Jiang Junchun Meng Jiansheng(Shangqiu Institute for Food and Drug Control,Shangqiu,Henan 476000) |
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| Abstract: | Objective To establish a HPLC method to determinate ferulic acid in fuyuekang capsules. Method The chromatographic system consisted of C18 column,using Methanol-5% Acetic acid glacial （22：78） as mobile phase.The content was detected at a waveleng of 322nm,the flow rate was 1.0ml？min-1. Results The curcumin have a good tincar rolatim in the range of 8.208～41.04μg？ml-1 （r=0.9999）, the average recovery was 99.07% and RSD=1.63% （n=6）. Conolusion The established method is accuracy ,sensitive and simple.It can be used for quality control of fuyuekang capsules. |
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| Keywords: | HPLC Ferulic acid Determination |
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