| 响应面法优化红花乙醇减压辅助提取工艺 |
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| 引用本文： | 王雅琪,何小汝,伍振峰,张小飞,兰继平,郑琴,杨明.响应面法优化红花乙醇减压辅助提取工艺[J].中国实验方剂学杂志,2016,22(3):5-8. |
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| 作者姓名： | 王雅琪 何小汝 伍振峰 张小飞 兰继平 郑琴 杨明 |
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| 作者单位： | 江西中医药大学, 南昌 330004,江西中医药大学, 南昌 330004,江西中医药大学, 南昌 330004,成都中医药大学, 成都 610075,江西中医药大学, 南昌 330004,江西中医药大学, 南昌 330004,江西中医药大学, 南昌 330004;成都中医药大学, 成都 610075 |
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| 基金项目： | 国家自然科学基金面上项目(81173565) |
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| 摘 要： | 目的:优化红花减压辅助提取的工艺参数,为该工艺的推广与应用提供参考。方法:以羟基红花黄色素A得率为指标,采用响应面分析法对乙醇体积分数、沸腾温度、提取次数、提取时间等参数进行考察,结合扫描电镜微观分析不同处理方式药材表面的微观形态。结果:最佳提取工艺为加20倍量50%乙醇于65℃提取2次,每次42 min。羟基红花黄色素A得率1.51%。结论:优选的减压提取工艺稳定可靠,羟基红花黄色素A得率显著高于传统回流提取法,提示减压提取法适合中药材中热敏性成分的提取。
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| 关 键 词： | 红花 羟基红花黄色素A 减压提取 扫描电镜 响应面分析 |
| 收稿时间： | 2015/6/24 0:00:00 |
Optimization of Vacuum-assisted Extraction Technology for Carthami Flos by Response Surface Methodology |
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| WANG Ya-qi,HE Xiao-ru,WU Zhen-feng,ZHANG Xiao-fei,LAN Ji-ping,ZHENG Qin and YANG Ming.Optimization of Vacuum-assisted Extraction Technology for Carthami Flos by Response Surface Methodology[J].China Journal of Experimental Traditional Medical Formulae,2016,22(3):5-8. |
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| Authors: | WANG Ya-qi HE Xiao-ru WU Zhen-feng ZHANG Xiao-fei LAN Ji-ping ZHENG Qin and YANG Ming |
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| Institution: | Jiangxi University of Traditional Chinese Medicine(TCM), Nanchang 330004, China,Jiangxi University of Traditional Chinese Medicine(TCM), Nanchang 330004, China,Jiangxi University of Traditional Chinese Medicine(TCM), Nanchang 330004, China,Chengdu University of TCM, Chengdu 610075, China,Jiangxi University of Traditional Chinese Medicine(TCM), Nanchang 330004, China,Jiangxi University of Traditional Chinese Medicine(TCM), Nanchang 330004, China and Jiangxi University of Traditional Chinese Medicine(TCM), Nanchang 330004, China;Chengdu University of TCM, Chengdu 610075, China |
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| Abstract: | |
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| Keywords: | Carthami Flos hydroxy safflower yellow A vacuum-assist extraction scanning electron microscope response surface analysis |
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