| HPLC测定全生白术散加味颗粒中橙皮苷的含量 |
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| 引用本文： | 陶莉莉,范宋玲,孙冬梅. HPLC测定全生白术散加味颗粒中橙皮苷的含量[J]. 中药新药与临床药理, 2003, 14(2): 115-116 |
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| 作者姓名： | 陶莉莉 范宋玲 孙冬梅 |
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| 作者单位： | 1. 广州中医药大学第一附属医院,广州,510405
2. 广东省中医研究所,广州,510095 |
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| 摘 要： | 目的：建立全生白术散加味颗粒中橙皮苷的测定方法。方法：采用高效液相色谱法测定橙皮苷的含量。结果：橙皮苷在0．22－1．1μg范围呈良好的线性关系，r=0.9998,平均回收率为103．0％，RSD为3．12％。结论：本方法准确，可用于该制剂的质量控制方法。
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| 关 键 词： | 全生白术散加味颗粒 化学分析 橙皮苷 高压液相色谱法 |
| 文章编号： | 1003-9783(2003)02-0115-02 |
| 修稿时间： | 2002-09-05 |
Content Determination of Hesperidin in Qiansheng Baizhusan Jiawei Granule by HPLC |
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| TAO Lili,FAN Songling,SUN Dongmei. Content Determination of Hesperidin in Qiansheng Baizhusan Jiawei Granule by HPLC[J]. Traditional Chinese Drug Research & Clinical Pharmacology, 2003, 14(2): 115-116 |
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| Authors: | TAO Lili FAN Songling SUN Dongmei |
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| Abstract: | Objective To establish a method for the determination of hesperidin content in Qiansheng Baizhusan Jiawei Granule (QBJG). Methods The content of hesperidin was determined by HPLC. Results Hesperidin showed a good linearity in the range of 0. 22-1.1ug(r = 0. 9998). The average recovery was 103. 0 % and RSD was 3. 12 %. Conclusion The methods are accurate and can be used for the quality control of QBJG. |
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| Keywords: | @ Qiansheng Baizhusan Jiawei Granule/chemistry Hesperidin/analysis HPLC |
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