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| 藏药螃蟹甲的化学成分研究 | |
| 引用本文： | 高咏莉,LIN Rui-chao,林瑞超,王钢力,赵浩如,高缘,边巴次仁.藏药螃蟹甲的化学成分研究[J].中药材,2007,30(10):1239-1242. |
| 作者姓名： | 高咏莉 LIN Rui-chao 林瑞超 王钢力 赵浩如 高缘 边巴次仁 |
| 作者单位： | 1. 中国药科大学,江苏南京210038;深圳市药品检验所,广东深圳518029 2. 中国药品生物制品检定所,北京,100050 3. 中国药科大学,江苏南京,210038 4. 西藏自治区药品检验所,西藏拉萨,850000 |
| 摘 要： | 目的:研究螃蟹甲地上部分的化学成分。方法:乙醇提取,氯仿、正丁醇依次萃取,硅胶柱层析分离纯化,通过理化常数和波谱分析鉴定化合物结构。结果:分离得到8个化合物,分别鉴定为8-乙酰山栀苷甲酯(8-ace-tylshanzhiside methyl ester)(1)、山栀苷甲酯(shanzhiside methyl ester)(2)、糙苏素(phlomiol)(3)、果糖丁苷(4)、sesamoside(5)、pulchelloside-Ⅰ(6)、木犀草素-7-O-β-D-葡萄糖苷(luteolin-7-O-β-D-glucopyranoside)(7)、胡萝卜苷(daucosterol)(8)。结论:上述化合物均为首次从螃蟹甲地上部分中分离得到。关键词螃蟹甲;化学成分 |
| 关 键 词： | 螃蟹甲 化学成分 |
| 文章编号： | 1001-4454（2007）10-1239-04 |
| 修稿时间： | 2007-04-19 |
Studies on the Chemical Constituents of Phlomis younghusbandii |
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| LIN Rui-chao.Studies on the Chemical Constituents of Phlomis younghusbandii[J].Jorunal of Chinese Medicinal Materials,2007,30(10):1239-1242. | |
| Authors: | LIN Rui-chao |
| Institution: | 1. Chinese Pharmaceutical University, Nanjing 210038, China; 2. Shenzhen City Institute for Drug Control, Shenzhen 518029, China ; 3. National Institute for Control of Pharmaceutical and Biological Products, Beijing 100050, China ; 4. Tibet Institute for Drug Control, Lasa 850000, China |
| Abstract: | OBJECTIVE: To study the chemical constituents of Phlomis younghusbandii. METHODS: Compounds were isolated from the ethanolic extract by silica gel column chromatography, and their structures were identified by physical and chemical evidences and spectral methods. RESULTS: Eight compounds were isolated and identified respectively as 8-acetylshanzhiside methyl ester (1), shanzhiside methyl ester (2), phlomiol (3), 2-butoxy-2-(hydroxymthyl) tetrahydro-2H-3,4,5-pyrantriol (4), sesamoside (5), pulchelloside-I (6), luteolin-7-O-beta-D-glucopyranoside (7) and daucosterol (8). CONCLUSION: All the compounds were isolated from the plant for the first time. |
| Keywords: | Phlomis younghusbandii Mukerjee Chemical constituents |
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