| 益肾康颗粒质量标准研究 |
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| 引用本文： | 吴星火,罗文汇,孙冬梅,李桂明.益肾康颗粒质量标准研究[J].广州医药,2009,40(1):62-64. |
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| 作者姓名： | 吴星火 罗文汇 孙冬梅 李桂明 |
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| 作者单位： | 1. 广东省第二中医院,510095
2. 广东省中医研究所,510095 |
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| 摘 要： | 目的对益肾康颗粒建立有效的质量控制方法。方法采用薄层色谱法对淫羊藿、白术、大黄、赤芍进行定性研究；采用薄层色谱扫描法测定了方中黄芪所含黄芪甲苷的含量。结果黄芪甲苷在0．54～4．32μg间呈现良好的线性关系，平均回收率为97．43％，RSD=1．08％；薄层色谱鉴别斑点清晰，无干扰，易分辨。结论所建立的方法简便、快速、准确，可有效地控制益肾康颗粒的质量。
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| 关 键 词： | 益肾康颗粒 质量标准 黄芪甲苷 薄层色谱扫描法 |
Quality standard of Yishenkang granules |
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| Institution: | Wu Xinghuo , Luo Wenhui , Sun Dongmei , et al.( 1. Guangdong Province 2nd Hospital of Traditional Chinese Medicinc , Gnangzhou, 510095 China; 2. Guangdong Province Institute of Traditional Chinese Medicine, Guangzhou, 510095 China) |
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| Abstract: | Objective To establish a method of quality control of Yishenkang granules. Methods Herba epimedii, Rhizmoa atractylodis macrocephalae, Radix et rhizoma rhei, Radix paeoniae rubra in Yishenkang granules were identified by TLC. Astragaloside Ⅳ in Yishenkang granules was determined by TLCS. Results The calibraction curve was linear in the range of 0. 54 -4. 32 μg, the average recovery was 97.4%, RSD = 1.08% ; the chromatographic spots were clear, without interference and easy to recognize. Conclusion The method was adoptable for the quality control of Yishenkang granules and the determination method of astragaloside Ⅳ is simple, rapid and accurate. |
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| Keywords: | Yishenkang granules Quality specification Astragaloside Ⅳ TLC-Scanning |
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