| HPLC法测定藤黄健骨丸中松果菊苷的含量 |
| |
| 引用本文： | 姜翔之,陈英红,罗浩铭,姜瑞芝. HPLC法测定藤黄健骨丸中松果菊苷的含量[J]. 中国药师, 2009, 12(4): 481-482 |
| |
| 作者姓名： | 姜翔之 陈英红 罗浩铭 姜瑞芝 |
| |
| 作者单位： | 1. 吉林大学中日联谊医院药剂科,长春,130051
2. 吉林省中医药科学院 |
| |
| 摘 要： | 目的：建立藤黄健骨丸中松果菊苷含量的HPLC测定方法。方法：色谱柱：DiamonsilC18（250mm×4．6mm，5μm），流动相：甲醇旬．1％甲酸（28．5：71．5），流速：1．0ml·min^-1，柱温：25℃，检测波长：330nm。结果：松果菊苷线性范围为0．18—1．84μg，r=0．9999，平均回收率为98．36％,RSD为0．56％（n=6）。结论：本法操作简便，结果准确。
|
| 关 键 词： | 藤黄健骨丸 松果菊苷 高效液相色谱法 |
Determination of Echinacoside in Tenghuang Jiangu Pills by HPLC |
| |
| Jiang Xiangzhi,Chen Yinghong,Luo Haoming,Jiang Ruizhi. Determination of Echinacoside in Tenghuang Jiangu Pills by HPLC[J]. China Pharmacist, 2009, 12(4): 481-482 |
| |
| Authors: | Jiang Xiangzhi Chen Yinghong Luo Haoming Jiang Ruizhi |
| |
| Affiliation: | Jiang Xiangzhi,Chen Yinghong, Luo Haoming, Jiang Ruizhi(1. Department of Pharmacy,Japan-China Union Hospital, Jilin University, Changchun 130051, China; 2. Jilin Academy of Traditional Chinese Medicine and Material Medical Sciences) |
| |
| Abstract: | Objective： To establish an HPLC method for the determination of echinacoside in Tenghuang Jiangu pills. Method ： A Diam6nsil C 18 （250 mm× 4.6mm,5μm） was used. The mobile phase consisted of methanol -0.1% formic acid （28.5：71.5） . The flow rate was 1.0ml·min^-1 and the column temperature was 25℃. The content was detected at a Wavelenght of 330nm. Result： The linear range was 0.18 - 1.84 μg for echinacoside （ r = 0. 9999）. The average recovery, rate was 98.36% with RSD of 0.56% （ n = 6）. Conclusion： The method was simple and accurate. |
| |
| Keywords: | Tenghuang Jiangu pills Echinacoside HPLC |
| 本文献已被 维普 万方数据 等数据库收录！ |
| 点击此处可从《中国药师》浏览原始摘要信息 |
|
点击此处可从《中国药师》下载全文 |
|
