| HPLC法测定益肾调经口服液中芍药苷的含量 |
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| 引用本文： | 陈静. HPLC法测定益肾调经口服液中芍药苷的含量[J]. 中国中医药现代远程教育, 2014, 0(2): 154-155 |
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| 作者姓名： | 陈静 |
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| 作者单位： | 河南省商丘市第一人民医院药剂科,商丘476000 |
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| 摘 要： | 目的建立HPLC法测定益肾调经口服液中芍药苷含量的方法。方法采用EclipseXDB-C18色谱柱,乙腈-0.1%磷酸溶液（14:86）为流动相;流速1.0ml·min-1;检测波长230nm。结果芍药苷在0.51652.066μg范围内线性关系良好（r=0.9995）,平均回收率为98.15%,RSD=0.91%（n=6）。结论本方法操作简便,专属性强,结果准确,可用于益肾调经口服液的质量控制。
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| 关 键 词： | 芍药苷 高效液相色谱法 含量测定 益肾调经口服液 |
Determination of Paeoniforin in Yishen Tiaojing Oral Liquid by HPLC |
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| Chen Jing. Determination of Paeoniforin in Yishen Tiaojing Oral Liquid by HPLC[J]. Chinese Medicine Modern Distance Education of China, 2014, 0(2): 154-155 |
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| Authors: | Chen Jing |
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| Affiliation: | Chen Jing (Pharmacy Department, Shangqiu First PeoplSs Hospital, Shangqiu, Henan Province,476000,China) |
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| Abstract: | Objective To establish a HPLC method of determination of paeoniforin in Yishen Tiaojing oral liquid. Method The chromatographic system consisted of C18 column, used acetonitrile- 0. 1% phosphate solution （14 ： 86） as mobile phase. The content was detected at a waveleng of 230nm,the flow rate was 1.0ml ·min^-1 . Results The paeoniforin have a good a linear relationship in the range of 0. 5165-2. 066μg（ r = 0. 9995）, the average recovery was 98. 15 % and RSD = 0. 91% （n = 6）. Conolusion The established method is accurate, sensitive and simple. It can be used for quality control of Yishen Tiaojing oral liquid. |
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| Keywords: | Paeoniforin HPLC Determination Yishen Tiaojing oral liquid |
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