| 虎耳草灌注剂的质量控制方法 |
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| 引用本文： | 郑岩,王红霞,陈随清. 虎耳草灌注剂的质量控制方法[J]. 中国中医药现代远程教育, 2014, 0(2): 150-151 |
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| 作者姓名： | 郑岩 王红霞 陈随清 |
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| 作者单位： | 河南中医学院药学院生药学科,郑州450008 |
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| 摘 要： | 目的 建立虎耳苹灌注剂的质量控制方法.方法 色谱柱为hypersil ODS （250mm×4.0mm、5μm）,流动相为甲醇-水（20∶80）,流速为1.0ml/n血,检测波长275nm,柱温30℃.结果 岩白菜素的进样量在0.0202～0.202μg之间与峰面积呈良好线性关系（R=0.9998）,平均回收率为102.45％,RSD=2.66％.结论 本方法灵敏、准确、重现性好,可用于虎耳草灌注剂的质量控制.
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| 关 键 词： | 虎耳草灌注剂 岩白菜素 HPLC 质量控制 |
Quality Control Method for Saxifraga Perfusion Agent |
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| Zheng Yan Wang Hongxia Chen Suiqing. Quality Control Method for Saxifraga Perfusion Agent[J]. Chinese Medicine Modern Distance Education of China, 2014, 0(2): 150-151 |
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| Authors: | Zheng Yan Wang Hongxia Chen Suiqing |
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| Affiliation: | Zheng Yan Wang Hongxia Chen Suiqing (Henan University of Traditional Chinese Medicine, Zhengzhou, Henan Province, 450008, China) |
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| Abstract: | Objective To establish a quality control method for the Saxifraga perfusion agent. Methods The analysis was performed on phe- nomenon hydro C18 column （250mm×4.0mm、5μm） , the mobile phase was MeOH-H20 （20 ： 80） with a flowtrate at 1.0ml/min, and detection wavelength at 275nm under column temperature 30℃. Results There was a good linear relationship when the sample size of berge- nin was at a range of 0. 0202μg-0. 404μg（R^2 = 0. 9998）, the recovery was 102.45 %, with RSD at 2. 66 %. Conclusion This method was simple, exact, and reproducible to be used for the quality control of the Saxifraga perfusion agent. |
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| Keywords: | Saxifraga perfusion agent Bergenin HPLC Quality control |
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