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HPLC法测定六味地黄口服液中马钱苷的含量
引用本文:单玉荣. HPLC法测定六味地黄口服液中马钱苷的含量[J]. 现代中药研究与实践, 2006, 20(6): 44-45
作者姓名:单玉荣
作者单位:安徽省药品检验所,安徽,合肥,230051
摘    要:目的研究六味地黄口服液中马钱苷的含量测定方法。方法高效液相色谱法,C18柱;流动相:四氢呋喃-乙腈-甲醇-0.05%磷酸(1∶8∶4∶87);检测波长为236 nm。结果平均加样回收率为100.33%,RSD=3.43%(n=6)。结论本法简便、准确、重复性好,可用于六味地黄口服液的质量控制。

关 键 词:六味地黄口服液  马钱苷  HPLC
文章编号:1004-2199(2006)06-0044-02
收稿时间:2006-07-09
修稿时间:2006-07-09

Determination of Loganin in Liuweidihuang Oral Liquid by HPLC
SHAN Yu-rong. Determination of Loganin in Liuweidihuang Oral Liquid by HPLC[J]. Research and Practice on Chinese Medicines, 2006, 20(6): 44-45
Authors:SHAN Yu-rong
Affiliation:Anhui Provincial Institute for Drug Control, Hefei 230051, China
Abstract:Objective To determine the content of loganin in Liuweidihuang oral liquid.Methods HPLC was carried out with C_(18 )column and tetrahydrofuran-acetonitrile-methanol-0.05%phosphoric acid(1∶8∶4∶87) as the mobile phase,the detection wavelength was at 236nm.Results The average recovery was 100.33%,RSD was 3.43%(n=6).Conclusion The method is simple,accurate with good reproducibility and can be used in quality control of Liuweidihuang oral solution.
Keywords:Liuweidihuang oral liquid  loganin  HPLC
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