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| 定量用三七总皂苷对照提取物的协作定值 | |
| 引用本文： | 鲁静,付凌燕,戴忠,张雯洁,祝明,曹红,顾立红,季申. 定量用三七总皂苷对照提取物的协作定值[J]. 中国药品标准, 2012, 13(3): 199-202 |
| 作者姓名： | 鲁静 付凌燕 戴忠 张雯洁 祝明 曹红 顾立红 季申 |
| 作者单位： | 1. 中国食品药品检定研究院,北京,100050 2. 中国食品药品检定研究院,北京,100050;吉林省吉林市药品检验所,吉林,132000 3. 云南省食品药品检验所,昆明,650011 4. 浙江省食品药品检验所,杭州,310004 5. 总后卫生部药品仪器检验所,北京,100071 6. 广州市药品检验所,广州,500160 7. 上海市食品药品检验所,上海,201203 |
| 摘 要： | 目的:建立定量用三七总皂苷对照提取物国家药品标准物质.方法:照<中国药典>2010年版一部三七总皂苷项下方法,以三七皂苷Rd、人参皂苷Rg1、人参皂苷Re、人参皂苷Rb1、人参皂苷Rd为指标,评价提取物备选原料的均匀性;5个实验室进行协作标定.结果:备选原料均匀性良好;对协作标定的测定结果进行统计分析确定了5种成分的标示值.结论:通过协作标定赋值,建立了首批定量用三七总皂苷对照提取物国家药品标准物质. |
| 关 键 词： | 对照提取物 三七总皂苷 标准物质 协作定值 |
The Collaborative Calibration of Quantitative Reference Extract of Notoginseng Total Saponins |
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| Lu Jing,Fu Lingyan,Dai Zhong,Zhang Wenjie,Zhu Ming,Cao Hong,Gu Lihong and Ji Shen. The Collaborative Calibration of Quantitative Reference Extract of Notoginseng Total Saponins[J]. , 2012, 13(3): 199-202 | |
| Authors: | Lu Jing Fu Lingyan Dai Zhong Zhang Wenjie Zhu Ming Cao Hong Gu Lihong Ji Shen |
| Affiliation: | 1. National Institute for Food and Drug Control, Beijing 100050; 2. Yunnan Institute for Food and Drug Control, Kunming 650011 ; 3. Zhefiang Institute for Food and Drug Control, Hangzhou 310004; 4. Institute for Drug and Instrument Control Health Dept, GLD of PLA, Beijing 100071 ; 5. Guangzhou Institute for Drug Control , Guangzhou 510000; 6. Shanghai Institute for Food and Drug Control, Shanghai 201210; 7. Jilin Institute for Food and Drug Control, Jinlin 132001 ) |
| Abstract: | Objective： To specify quantitative reference extract of notoginseng total saponins. Method： The uniformity of alternative raw materials was investigated by detecting the contents of notoginsenoside R1, ginsenoside Rg1 , ginsenoside Re, ginsenoside Rb1 and ginsenoside Rd using the method described under Notoginseng Total Saponins collected in Chinese Pharmacopoeia, Edition 2010. Five laboratories participate in the collaborative calibration test. Results： The alternative raw materials have good uniformity; the marked values of five components have been determined through the statistical analysis of the determining data provided by the five collaborative laboratories. Conclusion： The first batch of quantitative reference extract of Notoginseng Total Saponins had been specified based on the results of collaborative calibration. |
| Keywords: | reference extract notoginseng total saponins standard substance collaborative calibration |
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