| 高效液相法测定维C银翘片中马来酸氯苯那敏的含量 |
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| 引用本文： | 吴静.高效液相法测定维C银翘片中马来酸氯苯那敏的含量[J].现代中药研究与实践,2004,18(6):40-42. |
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| 作者姓名： | 吴静 |
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| 作者单位： | 安徽省芜湖市药品检验所,安徽,芜湖,241000 |
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| 摘 要： | 目的 建立维 C银翘片中马来酸氯苯那敏含量的 HPL C测定法。方法 采用十八烷基硅烷键合硅胶柱 ,流动相 :甲醇 -水 -冰醋酸 (2 0∶ 80∶ 2 .5 ) ,流速为 1.0 m L / min,检测波长 2 6 2 nm。结果 线性范围 :2 .5μg～ 10 0μg(r=0 .99999)。精密度 :RSD为 0 .0 6 % (n=5 ) .平均回收率为 10 0 .0 9%。结论 本法简便 ,快速 ,准确 ,可用于该药品的质量控制
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| 关 键 词： | 维C银翘片 马来酸氯苯那敏 高效液相色谱法 |
| 文章编号： | 1004-2199(2004)06-0040-03 |
| 修稿时间： | 2004年8月6日 |
Determination of Chlorphenamine Malea in Vitamin C Yinqiao Tablet by HPLC |
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| WU Jing.Determination of Chlorphenamine Malea in Vitamin C Yinqiao Tablet by HPLC[J].Research and Practice on Chinese Medicines,2004,18(6):40-42. |
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| Authors: | WU Jing |
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| Abstract: | Objective To develop a method for determination of Chlorphenamine Malea in Vitamin C Yinqiao Tablet with HPLC.Method A C18 silicon column was applied in HPLC. The stuffs for mobile phase were with methanol-water-acetic acid giacial (20∶80∶0.5), flow rate was 1.0mL/min, and detection wavelength was 262 nm.Result The linearity was obtained over the range of 2.5~100 μg(r=0.99999).(RSD 1.66%)The average recovery rate was 100.09%.Conclusion This method is simple, rapid, accurate and can be used for quality control for preparation of this medication. |
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| Keywords: | vitamin C Yinqiao tablet Chlorphenamine Malea HPLC |
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