| 刺五加叶挥发性化学成分的提取与气相色谱-质谱分析 |
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| 引用本文： | 张肖宁,孙妍,曹飞.刺五加叶挥发性化学成分的提取与气相色谱-质谱分析[J].中国新药杂志,2011(10). |
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| 作者姓名： | 张肖宁 孙妍 曹飞 |
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| 作者单位： | 黑龙江省食品药品检验检测所;黑龙江生物科技职业学院; |
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| 基金项目： | 黑龙江省中医药管理局科研项目(ZHY08-Z91) |
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| 摘 要： | 目的:比较不同提取方法对刺五加叶中挥发性化学成分的得率,并对其挥发性化学成分进行分析。方法:采用同时蒸馏萃取法(SDE)与常规提取法(水蒸气蒸馏法、溶剂法)对刺五加叶药材挥发性化学成分的提取收率进行比较研究,用GC/MS法对其挥发性化学成分进行分离鉴定,用峰面积归一化法得出各化学成分在挥发性组分中的相对百分含量。结果:共分离出51个成分,确认了其中39种化学成分,主要为萜类及其含氧衍生物(68.85%)和芳香族类化合物(6.32%),其中,(+)匙-叶桉油烯醇含量最高,达19.89%,其余依次为1甲-基-5亚-甲基-8-1甲-基乙基]-1,6环-癸二烯(7.02%)和1甲-基-1乙-烯基-2,4二-异丙烯基-环己烷(5.59%)等。结论:同时蒸馏萃取法是提取刺五加叶挥发性物质的优良方法。采用GC-MS法可以高效、适用、准确地分析、鉴定药材中挥发性物质的组成,对深入探索中药的药用价值具有积极的促进作用。
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| 关 键 词： | 刺五加叶 挥发性化学物质 GC/MS 同时蒸馏萃取法 |
Extraction and GC/MS analysis of volatile constituents from Acanthopanax senticosus (Rupr.et Maxim.) Harms leaf |
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| ZHANG Xiao-ning,SUN Yan,CAO Fei.Extraction and GC/MS analysis of volatile constituents from Acanthopanax senticosus (Rupr.et Maxim.) Harms leaf[J].Chinese Journal of New Drugs,2011(10). |
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| Authors: | ZHANG Xiao-ning SUN Yan CAO Fei |
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| Institution: | ZHANG Xiao-ning1,SUN Yan2,CAO Fei1(1 Heilongjiang Provincial Institute of Drug Control,Harbin 150001,China,2 Heilongjiang Vocational College of Biology Science and Technology,Harbin 150025,China) |
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| Abstract: | Objective: To determine the volatile constituents extracted from Acanthopanax senticosus(Rupr.et Maxim.) Harms leaf by different methods.Methods: Simultaneous distillation and solvent extraction(SDE),traditional hydrodistillation(HD) and solvent extraction were applied to analyze the volatile constituents of Acanthopanax senticosus(Rupr.et Maxim.) Harms leaf.The volatile constituents were identified by gas chromatography-mass spectrometry and the relative contents of the constituents were determined by an a... |
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| Keywords: | Acanthopanax senticosus(Rupr et Maxim ) Harms leaf volatile constituent GC/MS simultaneous distillation and solvent extraction |
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