| 气相色谱法测定小儿咽扁颗粒中冰片的含量 |
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| 引用本文： | 崔田.气相色谱法测定小儿咽扁颗粒中冰片的含量[J].海峡药学,2009,21(10):58-59. |
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| 作者姓名： | 崔田 |
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| 作者单位： | 安徽蚌埠市食品药品检验所,蚌埠233000 |
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| 摘 要： | 目的用毛细管气相色谱法建立测定小儿咽扁颗粒中冰片含量的方法。方法采用SUPELCOWAXTM-10毛细管柱（30m×0.53mm,1.0μm）,FID检测器,柱温140℃,以水杨酸甲酯为内标,按内标法计算冰片的含量。结果冰片在12.8μg-252μg（r=0.9997）范围内有较好线性关系,平均加样回收率为98.4%,RSD=0.6%（n=6）。结论该方法简便快速,结果准确。
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| 关 键 词： | 气相色谱法 小儿咽扁颗粒 冰片 |
Determination of borneol in Xiaoeryanbian granule by GC method |
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| CUI Tian.Determination of borneol in Xiaoeryanbian granule by GC method[J].Strait Pharmaceutical Journal,2009,21(10):58-59. |
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| Authors: | CUI Tian |
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| Institution: | CUI Tian(Anhui Bengbu Institute for Food and Drug Control, Bengbu 233000, China) |
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| Abstract: | OBJECTIVE To establish a capillary GC method for the determinatione of borneol in Xiaoeryanbian granule.METHODS The capillary column was used SUPELCOWAXTM-10（30m×0.53mm,1.0μm）,and the detector was FID.The column temperature was 140℃,and methylsalicylate was selected as internal standard.The assay of borneol was calculated by internal standard method.RESULTS Under this condition,the linearity relationship of borneol in the concentration range of 12.8μg～252μg was good（r=0.9997）.The average recovery was 98.4% with RSD of 0.6 % （n = 6）. CONCLUSION The method is convenient, rapid and accurate. |
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| Keywords: | GC Xiaoeryanbian granule Borneol |
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