| 跌打止痛微乳喷雾剂质量标准的研究 |
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| 引用本文： | 郭丽蓉,刘宏伟,周莉玲.跌打止痛微乳喷雾剂质量标准的研究[J].时珍国医国药,2011,22(5). |
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| 作者姓名： | 郭丽蓉 刘宏伟 周莉玲 |
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| 作者单位： | 广州中医药大学中药学院,广东,广州,510006 |
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| 摘 要： | 目的 建立跌打止痛微乳喷雾剂的质量标准.方法 采用薄层色谱法对处方中丁香罗勒油、八角茴香油、桉油、川芎、大黄、蛇床子、独活等7味药材进行定性鉴别,采用高效液相色谱法对制剂中的丁香酚和蛇床子素进行定量测定.结果 TLC法能定性检出丁香罗勒油、八角茴香油、桉油、川芎、大黄、蛇床子、独活,斑点清晰,且阴性对照无干扰;HPLC法测定丁香酚在0.051 5～0.927 mg/ml范围内线性关系良好;蛇床子素在5.20～93.6 μg/ml范围内线性关系良好.结论 所建立的定性、定量检测方法操作简便,结果准确可靠、重现性好,能有效地控制跌打止痛微乳喷雾剂的质量.
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| 关 键 词： | 跌打止痛微乳喷雾剂 薄层色谱 高效液相色谱 质量标准 |
Quality Standard of DieDaZhiTong Microemulsion Spray |
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| GUO Li-rong,LIU Hong-wei,ZHOU Li-ling.Quality Standard of DieDaZhiTong Microemulsion Spray[J].Lishizhen Medicine and Materia Medica Research,2011,22(5). |
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| Authors: | GUO Li-rong LIU Hong-wei ZHOU Li-ling |
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| Affiliation: | GUO Li-rong,LIU Hong-wei,ZHOU Li-ling*(Guangzhou University of Chinese Medicine,Guangzhou 510006,China) |
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| Abstract: | Objective To establish a quality standard for DieDaZhiTong Microemulsion Spray(DMS).Methods The qualitative identification of Oleum Ocimi Gratissimi,Anisestaroil,Eucalyptus Oil,Rhizoma Chuanxiong,Radix et Rhizoma Rhei,Fructus Cnidii,Radix Angelicae Pubescentis in DMS was carried out by TLC,and the contents of eugenol and osthole were determined by HPLC.Results The relevant spots of Oleum Ocimi Gratissimi,Anisestaroil,Rhizoma Chuanxiong,Radix et Rhizoma Rhei,Fructus Cnidii,Radix Angelicae Pubescentis on TLC ... |
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| Keywords: | DieDaZhiTong Microemulsion Spray TLC HPLC Quality standard |
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