| 刺山柑茎和叶的化学成分研究 |
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| 引用本文： | 杨涛,刘红娟,程雪梅,于富生,侴桂新,王长虹,王峥涛.刺山柑茎和叶的化学成分研究[J].西北药学杂志,2011,26(1):16-18. |
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| 作者姓名： | 杨涛 刘红娟 程雪梅 于富生 侴桂新 王长虹 王峥涛 |
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| 作者单位： | 1. 中药标准化教育部重点实验室,上海中医药大学中药研究所,中药新资源与质量标准综合评价国家中医药管理局重点研究室,上海市复方中药重点实验室,上海,201210;上海中药标准化研究中心,上海,201210
2. 新疆华圣元医药科技有限公司,新疆,乌鲁木齐,830011 |
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| 基金项目： | 上海市教育委员会科研项目资助课题，上海市重点学科建设资助项目 |
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| 摘 要： | 目的系统地研究刺山柑(Capparis spinosa)茎和叶的化学成分。方法采用硅胶、sephadex LH-20等色谱方法进行分离,再通过LC-MS、1H-NMR、13C-NMR等波谱数据进行结构鉴定。结果刺山柑茎和叶经体积分数85%的乙醇提取,从中分离鉴定了12个化合物,分别为:补骨脂素(psoralen,Ⅰ)、异补骨脂素(isopsoralen,Ⅱ)、对羟基苯甲酸乙酯(ethyl hydroxybenzo-ate,Ⅲ)、对羟基苯甲酸甲酯(methylparaben,Ⅳ)、反式肉桂酸(transcinnamic acid,Ⅴ)、苯甲酸(benzoic acid,Ⅵ)、对羟基苯甲酸(p-hydroxybenzoic acid,Ⅶ)、原儿茶酸(protocatechuic acid,Ⅷ)、山柰酚芸香苷(kaempfer-ol-3-O-rutinoside,Ⅸ)、芦丁(rutin,Ⅹ)、β-谷甾醇(β-sitosterol,Ⅺ)和β-胡萝卜苷(β-daucosterol,Ⅻ)。结论化合物Ⅰ~Ⅴ为首次从该属植物中分离得到。
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| 关 键 词： | 刺山柑 茎 叶 化学成分 |
The chemical constituents from stems and leaves of Capparis spinosa L. |
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| YANG Tao,LIU Hongjuan,CHENG Xuemei,YU Fusheng,CHOU Guixin,WANG Changhong,WANG Zhengtao.The chemical constituents from stems and leaves of Capparis spinosa L.[J].Northwest Pharmaceutical Journal,2011,26(1):16-18. |
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| Authors: | YANG Tao LIU Hongjuan CHENG Xuemei YU Fusheng CHOU Guixin WANG Changhong WANG Zhengtao |
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| Abstract: | Objective To study the chemical constituents of stems and leafs of Capparis spinosa L..Methods The compounds were separated and purified by column chromatography and their structures were analyzed by spectroscopic methods.Results Twelve compounds were isolated and purified,and their structures were determined as psoralen（Ⅰ）,isopsoralen（Ⅱ）,ethyl hydroxybenzoate（Ⅲ）,methylparaben（Ⅳ）,transcinnamic acid（Ⅴ）,benzoic acid（Ⅵ）,p-hydroxybenzoic acid（Ⅻ）,protocatechuic acid（Ⅷ）,kaempfer-ol-3-O-rutinoside（Ⅸ）,rutin（Ⅹ）,β-sitosterol（Ⅺ）,and β-daucosterol（Ⅻ）.Conclusion CompoundsⅠ-Ⅴ were isolated from Capparis for the first time. |
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| Keywords: | Capparis spinosa L Stem Leaf Chemical constituents |
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